Figure 1
Vertical (left) and horizontal (right) sections through the working electrode chamber of the fluorescence X-ray absorption spectroscopy spectroelectrochemical (XAS-SEC) cell. The control of solution flow is achieved using syringe pumps and 1/16-inch Teflon tubing. The inlet and outlet tubes of the WE are sealed with the aid of Teflon ferrules; a flanged seal was used for the CE tubing. |