Figure 1
(a) CAD drawing of the electrochemical cell and electrochemical cell head used for experimentation. All dimensions stated are in mm. (b) Three-dimensional schematic of the electrochemical cell and (c) photograph of the electrochemical cell setup on the beamline. 1: electrochemical cell head. 2: electrochemical cell. 3: `well' in which the working electrode is positioned. Under operation, LKE fills approximately half of the vessel, as shown in blue in (a). The positions of ancillary electrodes and thermocouple are also shown in blue. |