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Figure 2
Schematic of the capillary in situ electrochemical cell, including: (a) an overall schematic of the cell, containing the ep­oxy-aligned carbon fiber capillary working electrode connected to an electrolyte reservoir containing the counter electrode, and reference electrode. Electrolyte is recirculated via peristaltic pump to replenish the electrolyte species; (b) the components connecting the working electrode to the electrolyte reservoir; and (c) schematic of the interior of the working electrode, containing amorphous carbon powder support for the electrochemically active material.

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