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Figure 3
Photograph of a prototype in situ electrochemical cell with capillary working electrode in operation at 6-ID-D beamline at APS, showing (1) two-dimensional X-ray area detector, (2) photodiode, (3) carbon fiber capillary working electrode, (4) compression fitting, (5) electrolyte reservoir, and (6) ports with counter electrode, reference electrode and tubing for electrolyte recirculation.

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