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Figure 4
HE-XRD patterns for Fe–Ni LDH nanoparticles using two different in situ cell configurations: (a) conventional three-electrode half-cell without Fe–Ni LDH nanoparticles; (b) conventional three-electrode half-cell with Fe–Ni LDH nanoparticles; (c) aligned carbon fiber in situ cell without Fe–Ni LDH nanoparticles; and (d) aligned carbon fiber in situ cell with Fe–Ni LDH nanoparticles. HE-XRD from (a) and (b) were obtained at 11-ID-B (58.65 keV) while (c) and (d) were obtained at 6-ID-D (100 keV).

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