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Figure 6
(a) Pair distribution function calculated from in situ HE-XRD data for LiCoO2 in an aligned carbon fiber working electrode geometry for measurements taken under oxidizing and reducing potentials averaged over three cycles. (b) RMC fit of the reduction data in (a) using a bulk LiCoO2 starting structure. (c) A zoomed window of (a) highlighting changes measured under applied bias. (d) A species decomposed intensity from the reduction potential fit in (b) over the region highlighted in (c). Experiments were performed at the 6-ID-D beamline at APS.

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