An electrochemical cell with sapphire windows for operando synchrotron X-ray powder diffraction and spectroscopy studies of high-power and high-voltage electrodes for metal-ion batteries

Drozhzhin, O.A.; Tereshchenko, I.V.; Emerich, H.; Antipov, E.V.; Abakumov, A.M.; Chernyshov, D.

doi:10.1107/S1600577517017489

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Figure 3
Results of sequential Rietveld refinement. (a) The mass fraction of each phase. (b) Their unit-cell parameters. (c) The corresponding E–C curves collected during charge (C/2 rate) and discharge (10C rate). The notations stand for the three distinct Li_1–xFe_0.5Mn_0.5PO₄ phases: Li-rich (LFMP, x > 0.8), intermediate (L05FMP, 0.3 < x < 0.8) and Li-poor (FMP, x < 0.3).

JOURNAL OF
SYNCHROTRON
RADIATION

ISSN: 1600-5775

Volume 25| Part 2| March 2018| Pages 468-472

https://doi.org/10.1107/S1600577517017489

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