Smaller capillaries improve the small-angle X-ray scattering signal and sample consumption for biomacromolecular solutions

Schroer, M.A.; Blanchet, C.E.; Gruzinov, A.Y.; Gräwert, M.A.; Brennich, M.E.; Hajizadeh, N.R.; Jeffries, C.M.; Svergun, D.I.

doi:10.1107/S1600577518007907

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Figure 3
Single SAXS curves I(s) versus s for the lysozyme sample in (a) d_i = 1.7 mm and (b) d_i = 0.9 mm capillaries at a total volume flow rate Q = 20 µl s⁻¹. With increasing exposure time, the scattering intensity at low s increases due to the formation of radiation-induced aggregates, especially in the larger-diameter capillary.

JOURNAL OF
SYNCHROTRON
RADIATION

ISSN: 1600-5775

Volume 25| Part 4| July 2018| Pages 1113-1122

https://doi.org/10.1107/S1600577518007907

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