Figure 9
(a) Least-squares model curve fitting to the k3-weighted Rh K-edge EXAFS spectrum of solid 10, i.e. the reaction product of Rh2(AcO)4 with excess Na3(DTLA); the contributions from the Rh—S, Rh⋯Rh and Rh—S—Rh—S (nleg = 4; along the linear S—Rh—S entities) scattering paths are shown separately; (b) the corresponding Fourier transforms. |