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Figure 2
(a) CAD of the in situ electrochemical cell. (b) A photograph of the in situ electrochemical cell assembly installed during HEXS data acquisition and consisting of electrolyte reservoir, in situ cell body with syringe pump, WE, RE, CE, holder for RE, and mounting stage including Newport Kinematic base, Thorlab rail carrier and dovetail optical rail. Polyimide film (yellow) holds electrolyte. (c) Magnification of the WE and reference side during electrolysis after 1 h of electrolysis. (d) Scaled, schematic side-view drawing showing the horizontal scanning width of X-ray on IZO/Au/GCA electrode. The size of the incoming X-ray beam is 500 mm (width) by 300 mm (height) as indicated by the red rectangular box in (d).

Journal logoJOURNAL OF
SYNCHROTRON
RADIATION
ISSN: 1600-5775
Volume 26| Part 5| September 2019| Pages 1600-1611
https://doi.org/10.1107/S1600577519007240
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