A versatile nanoreactor for complementary in situ X-ray and electron microscopy studies in catalysis and materials science

Fam, Y.; Sheppard, T.L.; Becher, J.; Scherhaufer, D.; Lambach, H.; Kulkarni, S.; Keller, T.F.; Wittstock, A.; Wittwer, F.; Seyrich, M.; Brueckner, D.; Kahnt, M.; Yang, X.; Schropp, A.; Stierle, A.; Schroer, C.G.; Grunwaldt, J.-D.

doi:10.1107/S160057751900660X

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Figure 5
Ptychography images from thermal annealing of np-Au under a He environment. Overview scans: (a) before and (b) after thermal annealing. Highlighted area in (a) and (b) shown: (c) at 293 K, (d) 923 K after 0 min, (e) 923 K after 15 min and (f) 923 K after 30 min. Darker intensity in phase maps indicates areas rich in Au, while brighter voids indicate annealing and absence of Au ligaments. Pt glue from FIB is visible as intense features in the corners of (a) and (b).

JOURNAL OF
SYNCHROTRON
RADIATION

ISSN: 1600-5775

Volume 26| Part 5| September 2019| Pages 1769-1781

https://doi.org/10.1107/S160057751900660X

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