view article
Figure 8
Results of the pressure test performed at 74 K and 204 K with blue squares and red dots, respectively. Pressure in the cell in GPa as a function of the pressure in the membrane in bars. The first determined using the ruby fluorescence technique, the second regulated using a GE Druck PACE5000 gas controller. The cell was prepared using 4:1 methanol:ethanol as PTM and it was closed initially at 1 GPa. The test was performed in the first place at 74 K reaching a maximum pressure close to 20 GPa. Then the pressure in the membrane was released and the test was repeated at 204 K.

Journal logoJOURNAL OF
SYNCHROTRON
RADIATION
ISSN: 1600-5775
Volume 27| Part 2| March 2020| Pages 351-359
https://doi.org/10.1107/S1600577519016308
Follow J. Synchrotron Rad.
Sign up for e-alerts
E-alerts
Follow J. Synchrotron Rad. on Twitter
Twitter
Follow us on facebook
Facebook
Sign up for RSS feeds
RSS