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Figure 2
Selection of GISAXS patterns at different processing times during the thermal annealing at 180°C. The dashed vertical and horizontal lines indicate the qy and qz main peak position for the further analysis using line cut profiles. After reaching 180°C (t = 0 s) with a ramp rate of 50°C min−1, GISAXS patterns were collected with a frame rate of 1 frame of 37 ms every 60 s. GISAXS patterns showed a clear scattering evolution of the BCP film during the isothermal process: lobe sharpness and the appearance of vertical second-order peaks along qz were indicative of an increase in the long-range structure of the BCP.

Journal logoJOURNAL OF
SYNCHROTRON
RADIATION
ISSN: 1600-5775
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