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Figure 13
Temperature-programmed XPS spectra during heating of a Pd foil in 1 mbar O2. (a) Pd 3d 2D plot of binding energy versus temperature; (b) Pd 3d spectra at selected temperatures (average of three spectra centred at the respective temperature). (c) O 1s 2D plot binding energy versus temperature. (d) O 1s/Pd 3d3/2 spectra at selected temperatures (average of five spectra centred at the respective temperature). Photon energy = 750 eV; exit slit = 0.05 mm; pass energy = 10 eV.

Journal logoJOURNAL OF
SYNCHROTRON
RADIATION
ISSN: 1600-5775
Volume 27| Part 5| September 2020| Pages 1153-1166
https://doi.org/10.1107/S1600577520009157
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