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![[Figure 2]](gb5115fig2mag.jpg)
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Figure 2
The annealing temperature profile as a function of time. Changes in the temperature step size are marked by the red dashed lines. (a) Tcalibrated was raised from room temperature to 209°C using ∼50°C steps with a ramp rate of 2°C min−1. (b) From 209°C to 409°C, ∼5°C steps were used with a ramp rate of 50°C min−1. Finally, from 409°C to 587°C, ∼20°C steps were used with a ramp rate of 50°C min−1. The ramp rate reported here is with respect to Tmeasured and was lower in (a) to ensure that the alignment macro could update the positions of the reflections for larger temperature steps. |
![[Figure 2]](gb5115fig2.jpg)
 | JOURNAL OF SYNCHROTRON RADIATION |
ISSN: 1600-5775
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