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Figure 7
Reflection-specific r matrices between uhkl(r) for different temperatures. The difference in r values corresponds to structural evolution. The (002) reflection for crystal A shows an abrupt r change after 410°C, suggesting the abrupt removal of most defects. This is less evident in the [(11\bar{1})] reflection for crystal B, which shows many subtle structural changes as a function of temperature. The red dashed lines indicate where the temperature sampling changed. Black arrows represent the most noticeable changes in displacement.

Journal logoJOURNAL OF
SYNCHROTRON
RADIATION
ISSN: 1600-5775
Volume 28| Part 2| March 2021| Pages 550-565
https://doi.org/10.1107/S1600577520016264
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