Figure 3
Correlative XAS–XEOL images recorded on a ZnO crystallite agglomerate of the ZnO-L sample. (a) False-color many-energy STXM image showing XNLD orientation contrast retrieved through SiVM-NNLS analysis. The white parallelogram indicates the region at which XEOL data were recorded. (b) Zn L-edge XANES retrieved from the many-energy STXM map at the locations indicated by the white crosses. (c) False-color XEOL image, obtained by integrating the band gap emission (352–390 nm, red channel), green trap state emission (455–500 nm, green channel) and blue trap state emission (399–442 nm, blue channel) collected with the excitation energy tuned to 1050 eV. (d) XEOL spectra retrieved from the hyperspectral XEOL map at the locations indicated by the white crosses. |