Beamline K11 DIAD: a new instrument for dual imaging and diffraction at Diamond Light Source

Reinhard, C.; Drakopoulos, M.; Ahmed, S.I.; Deyhle, H.; James, A.; Charlesworth, C.M.; Burt, M.; Sutter, J.; Alexander, S.; Garland, P.; Yates, T.; Marshall, R.; Kemp, B.; Warrick, E.; Pueyos, A.; Bradnick, B.; Nagni, M.; Winter, A.D.; Filik, J.; Basham, M.; Wadeson, N.; King, O.N.F.; Aslani, N.; Dent, A.J.

doi:10.1107/S1600577521009875

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Figure 7
LaB₆ calibration pattern collected at three vertical locations of a 0.3 mm-diameter capillary during rotation, at an incident beam energy of 24.69 keV. The sum of the three raw images is shown in (a) with the inset (white) showing a region of the (100) reflection at a higher magnification. The azimuthally integrated patterns are shown in (b). The intensities have been scaled relative to the maximum value obtained for the (110) reflection for each pattern. The inset shows the (100) peak in more detail including the expected position for a d-spacing of 4.15692 Å. The alignment across all locations shows that the automated calibration procedure compensating for the moving beam is effective and instrumental artefacts can be corrected for.

JOURNAL OF
SYNCHROTRON
RADIATION

ISSN: 1600-5775

Volume 28| Part 6| November 2021| Pages 1985-1995

https://doi.org/10.1107/S1600577521009875

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