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Figure 13
Powder diffraction pattern from a 0.25 mm diameter capillary filled with LaB6 reference powder from NIST measured at 17.94 keV (blue points). Two images were recorded at two detector positions for a total acquisition time of 2 × 10 s and the selected threshold calibration of the detector was with beam mode and SLOW settings. The red line is the whole pattern structural refinement performed using the NIST reference values. The inset shows a magnification of two peaks at high angles.

Journal logoJOURNAL OF
SYNCHROTRON
RADIATION
ISSN: 1600-5775
Volume 29| Part 1| January 2022| Pages 180-193
https://doi.org/10.1107/S1600577521012492
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