In situ beam reduction of Pu(IV) and Bk(IV) as a route to trivalent transuranic coordination complexes with hydroxypyridinone chelators

Carter, K.P.; Wacker, J.N.; Smith, K.F.; Deblonde, G.J.-P.; Moreau, L.M.; Rees, J.A.; Booth, C.H.; Abergel, R.J.

doi:10.1107/S1600577522000200

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Figure 3
EXAFS data and fit (top) and Fourier transform of the k-space data and fit (bottom) for Bk(III)-343-HOPO and Pu(III)-343-HOPO. (a, b) Free fit, except fixed multiple scattering peak amplitudes, for Bk(III)-343-HOPO. (c, d) Pu(III)-343-HOPO fit with multiple scattering paths fixed. Error bars for the raw, unfiltered data are estimated as the standard deviation of the mean between individual traces. Note that comparison between fit and data in k-space should be to the filtered data, which has been back-transformed over the fit range.

JOURNAL OF
SYNCHROTRON
RADIATION

ISSN: 1600-5775

Volume 29| Part 2| March 2022| Pages 315-322

https://doi.org/10.1107/S1600577522000200

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