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Figure 5
The locations of the centre and edge areas where XRD data were collected as a function of temperature. (a) An optical microscope image of Pt powder on the bottom chip showing the locations of the thinned areas for electron microscope measurements. (b) A Mo map of the heater spiral with inset Pt maps from (red box) centre and (blue box) edge areas. (c) An example XRD pattern from the mapped area.

Journal logoJOURNAL OF
SYNCHROTRON
RADIATION
ISSN: 1600-5775
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