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Figure 4
Diffraction pattern of FeH at 39 GPa with H2 as PTM loaded into the amorphous metal insert in a Re gasket. (a) 2D diffraction pattern without any evident contribution from the gasket material. The hydrogen signal is barely visible due to its low scattering power. Diamond Bragg peaks are masked with red markers. (b) The corresponding integrated 1D diffraction pattern including the indexing of FeH peaks. The insert shows the reconstruction of the phase distribution obtained from the analysis of the 2D pXRD map produced by sample scanning. We indicate the position of FeH and ruby in the sample chamber surrounded by amorphous metal. The boundary of the amorphous metallic material can be clearly seen.

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SYNCHROTRON
RADIATION
ISSN: 1600-5775
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