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Figure 3
Error is introduced into the PDF if highly absorbing samples are not diluted. (a) Comparison in baseline between the empty borosilicate capillary, SiO2, diluted (Cu + SiO2) and undiluted Cu; (b) the diffracted intensities for undiluted Cu at high angles are stronger than what the structure model for Cu would predict; (c) S(Q); and (d) F(Q) showing the difference in background subtraction of Cu.

Journal logoJOURNAL OF
SYNCHROTRON
RADIATION
ISSN: 1600-5775
Volume 30| Part 2| March 2023| Pages 327-339
https://doi.org/10.1107/S1600577522011614
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