Figure 1
Scheme of the experimental setup developed for combined X-ray photon correlation spectroscopy and nano-calorimetry. The X-ray beam is focused onto a spot a few micrometres in size on the sample mounted on the calorimeter chip. The scattered radiation is collected with a 2D detector downstream of the experimental chamber. The chip's electrical contacts are connected to the body of the calorimeter in order to control the temperature and perform thermal cycles (heating/cooling). Inset: zoom of the chip holder with illustration of the replicated contacts to connect the chip to the calorimeter. |