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Figure 5
Heat flow measured for a sample of Pd42.5Cu30Ni7.5P20 with the Flash DSC 2+ calorimeter. (a) Raw data for a heating rate of β = 1000 K s−1 in standard conditions (full line), i.e. measured at ambient N2 pressure in the calorimeter chassis, and in vacuum inside the P10 experimental chamber (dashed line). (b) The thermograms of panel (a) are reported after data correction. Inset: zoom of the glass transition region, highlighting a small temperature difference (ΔT = 1.3 K) between the two thermograms.

Journal logoJOURNAL OF
SYNCHROTRON
RADIATION
ISSN: 1600-5775
Volume 31| Part 3| May 2024| Pages 557-565
https://doi.org/10.1107/S1600577524002510
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