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Figure 1
Design of the in situ XRD/XAS electrochemical cell. (a) Exploded view showing different components of the cell: (1) front rotating cap 1 (large), (2) front rotating cap 2 (small), (3) housing structure, (4) main component of the cell, (5) Kapton membrane, (6) back rotating cap 2 (small), (7) back rotating cap 1 (large) and (8) sample stage. (b) 3D rendering showing the intricate design of the cell's cross-sectional architecture. (c) Scheme for 2D XRD measurement. (d) Scheme for XAS measurement in both fluorescence and transmission modes. (e) Cross-sectional view showing the collection angle of X-ray signals. (f) XRD pattern of an LaB6 electrode. (g) Photograph of the fabricated cell.

Journal logoJOURNAL OF
SYNCHROTRON
RADIATION
ISSN: 1600-5775
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