Design and application of an electrochemical cell for operando X-ray diffraction and absorption studies for electrocatalysts

Chen, J.; Li, Z.; Zeng, H.; Deng, L.; Gu, L.; Wang, C.; Yang, C.; Sun, D.

doi:10.1107/S1600577525005612

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Figure 5
(a)–(b) Two-dimensional XRD patterns collected by the Pilatus3R 1M X-ray detector (a) at OCV and (b) at 1.7 V during the operando XRD measurement. (c)–(d) The derived 2θ XRD profiles of LiCoO₂ (c) at OCV and (d) at 1.7 V. (e) Illustration of the crystal structure changes during OER.

JOURNAL OF
SYNCHROTRON
RADIATION

ISSN: 1600-5775

Volume 32| Part 5| September 2025| Pages 1272-1281

https://doi.org/10.1107/S1600577525005612

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