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Figure 7
Two-dimensional diffraction patterns of the b.c.c.-Fe taken during heating of the α phase (ac) and solidification of the δ phase (bf) on stationary and spinning samples. The off-center geometry captured by the PILATUS detector during the cycle shown in Fig. 6[link] is compared with the symmetrical pattern acquired with the XRD 1621 detector during a similar thermal cycle. The sensitive areas of both detectors are displayed to scale. A magnified view of the areas indicated by the black boxes is shown in the corresponding bottom panels.

Journal logoJOURNAL OF
SYNCHROTRON
RADIATION
ISSN: 1600-5775
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