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Figure 8
Intensity distributions along the (110) (a) and (200) (b) rings of an α-Fe pattern from Fig. 7[link](c) as a function of azimuthal angle χ. Upper panels compare profiles integrated over the full χ range (red) with profiles at selected azimuthal angles (black); the asymmetry of the integrated profile reflects limited statistics due to a reduced χ range measured in the current geometry. FWHM values from deconvoluted profiles at selected χ angles are compared with calculated resolution functions for different effective sample sizes (c). Maximum inter-peak distance measured across the χ range compared with the sum of the main broadening contributions (d).

Journal logoJOURNAL OF
SYNCHROTRON
RADIATION
ISSN: 1600-5775
Volume 33| Part 4| July 2026|
https://doi.org/10.1107/S1600577526003541
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