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Figure 3
(a) Three-dimensional (3D) schematic model of the reaction cell showing key components: (1) gas inlet; (2) gas outlet; (3) thermocouple, positioned to monitor the temperature accurately; (4) resistive coils, heating to desired reaction temperatures; (5) capillary, allowing access for in situ measurements in continuous gas flow conditions; and (6) metal gasket face seal fittings, ensuring a hermetic and high-pressure-resistant seal. (b) Photograph of the assembled reaction cell, illustrating the physical arrangement, corresponding directly to the 3D model in (a).

Journal logoJOURNAL OF
SYNCHROTRON
RADIATION
ISSN: 1600-5775
Volume 33| Part 4| July 2026|
https://doi.org/10.1107/S1600577526003656
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