Disodium Bis(malonato)cuprate(II) Dihydrate

1-Benzoyl-5-hy­droxy-2,4-di­phenyl-5-propionyl­oxy-3-imidazoline

(+)-(2S,3S,4S,5S)-2-Benzyl-N-(tert-butyloxycarbonyl)-3-hy­droxy-4,5-di­methylpyrrolidine at 143K

(2S,3R,4R,5R,SS)-2-Benzyl-3-hy­droxy-5-{N-[(S)-1-hy­droxy-3-methylbut-2-yl]-4-methylphenylsulfonimidoylmethyl}-4-methyl-1-(4-methylphenylsulfonyl)pyrrolidine at 140K

4-Bromo­methyl-7,8-benzocoumarin

Bis(2-methylbenzyl cyanide) Tetra­cyano­benzene

7-(4-Nitro­phenyl)-7-azabi­cyclo[4.1.0]heptane

Lithium Vanadium Metasilicate, LiVSi₂O₆

The structure of the pyroxene LiVSi₂O₆ is composed of infinite chains of edge-sharing VO₆ octahedra linked together by corner-sharing SiO₄ tetrahedra.

YBa(Cu_1.10Co_0.90)O₅, Prepared from YBa₂Cu₃O₇

The structure of YBa(Cu_1.10Co_0.90)O₅ is constructed from the four bound layers BaO–(Cu,Co)O₂–Y–(Cu,Co)O₂. The mixed (Cu,Co) site atoms form distorted square-pyramidal pair-layers based on (Cu,Co)₂O₉, linked through their basal and apical O atoms.

The First Cadmium Rare Earth Borates CdLn[B₅O₁₀] with Ln = La, Sm, Eu

The crystal structure of CdLn[B₅O₁₀] (Ln = La, Sm, Eu) contains planar infinite two-dimensional [B₅O₁₀]⁵⁻ polyborate anions perpendicular to [101], separated by LnO₁₀ polyhedra and Cd₂O₁₀ octahedral dimers. Three out of the five B atoms are four-coordinate, the other two have trigonal planar coordination.

Structure d'un Monophosphate Synthétique de Magnésium et de Sodium: Mg₃Na₃(PO₄)₃

The structure of the monophosphate Mg₃Na₃(PO₄)₃ contains three kinds of Mg–O polyhedra which form two types of infinite chain parallel to the shortest axis of the cell. The chains are connected with PO₄ tetrahedra by corner-sharing to form a framework. The 1/3 substructure appears along the longest axis of the cell.

Mixed Ba_5.24Sr_0.76Mg₇F₂₆

The mixed compound (Ba_1-δSr_δ)₆Mg₇F₂₆ has a structure which can be described as comprising perovskite-like blocks and rutile-related parts. Only one of the two Ba sites is partially (30%) replaced by Sr.

A New Zinc Pyrovanadate, Zn₃(OH)₂V₂O₇.2H₂O, from X-ray Powder Data

Rietveld refinement of a new zinc divanadate, Zn₃(OH)₂V₂O₇.2H₂O, shows that it has a porous framework structure assembled from layers of Zn–O octahedra joined by pyrovanadate groups. Water molecules fill the large cavities.

Ca₄PtO₆

The structure of Ca₄PtO₆ consists of chains of alternating face-sharing Pt-centered octahedra and distorted Ca-centered trigonal prisms running parallel to the c axis, with the remaining Ca²⁺ ions arranged between the columns.

Dibarium Magnesium Phosphate

Ba₂Mg(PO₄)₂ is isostructural with Ba₂Ni(PO₄)₂ and consists of a three-dimensional framework of MgO₆ octahedra and PO₄ tetrahedra generating tunnels which accommodate Ba atoms.

A New Structural Variation of Nb₃YX₇ Compounds: Monoclinic Nb₃SI₇

Monoclinic Nb₃SI₇ crystallizes in a novel two-dimensional structure. The structure comprises [Nb₃SI₁₀]³⁻ clusters which contain Nb triangles bicapped by μ₃-I and μ₃-S atoms. The clusters are linked to form dimeric units and these dimers are cross-linked to form layers of composition Nb₃SI₇.

Fe₃W₃N: a Rietveld Refinement Using X-ray Powder Diffraction

Fe₃W₃N is isostructural with Westgren's cubic η-carbide structure and contains two sets of coordination polyhedra: NW₆ octahedra, which share corners as in the pyrochlore structure, and Fe₈ stellae quadrangulae, which also share corners on a structural lattice separate from that formed by the NW₆ octahedra.

Cerous Silver Nitrate, Ag₆Ce(NO₃)₉

The structure of Ag₆Ce(NO₃)₉ consists of icosahedral [Ce(NO₃)₆]³⁻ ions located in a framework of eightfold Ag polyhedra.

Eu₂Si₅N₈ and EuYbSi₄N₇. The First Nitridosilicates with a Divalent Rare Earth Metal

The crystal structures of Eu₂Si₅N₈ and EuYbSi₄N₇, which both contain highly condensed Si–N networks, are reported.

Potassium Cobalt Aluminium Mixed Phosphate, K(Co^II,Al)₂(PO₄)₂

The structure of K(Co^II,Al)₂(PO₄)₂ is built up from corner- sharing (Co/Al)O₄ and PO₄ tetrahedra to form intersecting tunnels running parallel to the unit-cell axes, with K atoms situated in the tunnels.

β-(1,10-Phenanthroline)(1,3-propanedi­amine-N,N'-di­acetato)cobalt(III) Chloride Trihydrate

Bis(3,5-di­methylpyrazole-N²)(N-salicylideneglycinato-O,N,O')copper(II)

A Stable Sulfonato–Cobalt(III) Complex: Δ-[Co{OS(O)₂CH₂CH₂NH₂-N,O}(en)₂](ClO₄)₂

Mono­ammonium Bis(D-penicillaminato-S)aurate(I) 3.667-Hydrate

cyclo-Hexa­kis­[(2,4,6-triiso­propylthiophenolato-S:S)gold(I)] Di­ethyl Ether Solvate

A New Perylene Salt: Diperylenium(1+) Bis[quinoxaline-2,3-di­thiolato(2 –)-S,S']cuprate(III)

A Nickel(II) Compound with a Tetradentate Di­amine–Di­imine Ligand, (2,4,6,9,11-Penta­methyl-5,8-di­azadodeca-4,8-diene-2,11-di­amine)nickel(II) Tetra­chlorozincate

Accurate Redeterminations of 1,1'-Di­benzoylferrocene and (4-Nitro­phenyl)ferrocene

(1'-Benzoylferrocenyl)di­phenylmethanol; a Centrosymmetric ⁴₄(16) Dimer Generated by C—H⋯O Hydrogen Bonding

(1,4,7,11,13-Penta­aza­cyclohexa­decane-κ⁵N)(perchlorato-κO)nickel(II) Perchlorate

Chloro(1,4,7,11-tetra­aza­cyclo­tetra­decane-N,N',N'',N''')zinc(II) Perchlorate

Di-μ-acetato-bis­[di­carbonyl(pyrazole)ruthenium(I)] and Di-μ-acetato-bis­[di­carbonyl(3,5-di­methylpyrazole)ruthenium(I)]

A New Modification of 1,1'-Bis(di­phenylphosphine oxide)ferrocene at 173K

Redetermination of Bis(2-aminopyrimidinium) Tetra­bromocopper(II) at 200 and 100K

The 1:1 Antimony Trichloride Adduct of Chlorobis(2,6-di­methylpiperidin-1-yl)phosphine Oxide

Piperidinium Di­azidotri­phenylstannate and Quinuclidinium Di­azidotri­phenylstannate

Di­bromobis(η⁵-penta­methylcyclo­pentadienyl)thorium(IV)

Disodium Hexadecahydrate Diprotonated Form of 1,4,8,11-Tetra(2-carb­oxy)ethyl-1,4,8,11-tetra­aza­cyclo­tetra­decane (H₂TETP)²⁻ at 110 K

Octa­carbonyl-μ-chloro-μ-di­cyclo­hexylphosphido-dimanganese

Polymeric Aquatri-μ-chloro-(tetra­hydro­furan-O)lanthanum(III)

A Chromium(III) 2,2'-Bi­pyrimidine (bipym) Complex, (Et₄N)[Cr(NCS)₄(bipym)]

Mononuclear Indium and Gallium Tetra­chlorocatecholate Complexes

Polysulfonylamines. XCIII. (1,2-Benzenedi­sulfonylimido-O)(1,4,7,10-tetraoxa­cyclodo­decane-κ⁴O)lithium

Polysulfonylamines. XCV. (1,2-Benzenedi­sulfonylimido-N,O)(1,4,7,10,13-pentaoxa­cyclo­penta­decane-κ⁵O)sodium

Di­chloro[2,3,5,6-tetra(2-pyridyl)pyrazine]copper(II), [CuCl₂(C₂₄H₁₆N₆)]

Cadmium Glutamate Dihydrate

Dual Behaviour of Acetylacetonate Anions in the Hydrogen-Bonded Supramolecular Structure (Acetylacetonato-O,O')[trans-(1R,2R)-di­amino­cyclo­hexane-N,N']platinum(II) Acetylacetonate

Doubly Interpenetrating Three-Dimensional Framework Structure of trans-[Cd(dppn)₂{Ag(CN)₂}₂]_n [dppn = 1,3-Di(4-pyridyl)propane]

Three Complexes of a [2.2]Cryptahemispherand

An Na⁺ Complex and a Bis-BH₃ Complex of a [1.1]Cryptahemispherand

A K⁺ Complex of a [2.1]Cryptahemispherand at 295K

Two Isomeric [2.1]Cryptahemispherand Di­amides

(±)-2,3-Di­hydro-3-oxo-1H-indene­carboxylic Acid: Hydrogen-Bonding Patterns in a γ-Keto Acid and its Monohydrate

2,4,5-Tri­methylbenzoic Acid

Bis(tri­methylsilyl)acetylene

Pyrrole and a Co-crystal of 1H- and 2H-1,2,3-Triazole

1-Ethyl-3-hy­droxy-4,4-di­methyl-2-pyrrolidone

A New Modification of Bis(di­phenylphosphino)methane Diselenide

8-Hy­droxy-4-methyl-9-phenylthio-7,8,9,10-tetra­hydro-7,8-benzocoumarin

5-Amino-1,6-di­methyl-1,2-di­hydroquinolin-2-one Monohydrate

Bis(3,4-di­methoxybenzyl) Ether and Tetra­meth­oxy-4,4'-(2,3-di­methyltetra­methylene)dipyrocatechol

Substituted Methoxybenzene Derivatives: C₈H₉NO₄, C₉H₁₁NO₅ and C₁₃H₁₈O₄

5,6,8-Tri­chloro-4-phenyl-3,4-di­hydroquinolin-2(1H)-one

6-n-Butylace­naphtho[1,2-b]benzo[h]quinoline

N-(4-Nitro­phenyl)-trans-2-amino­cyclo­hexanol

Two Cyclo­tetrasiloxanes at 143K

A Tetragonal-Looking But Twinned Orthorhombic Structure

Methyl 3',6'-Bis(chloro­methyl)-2,2'-di­meth­oxy-1,1'-bi­naphthalene-3-carboxylate

A 2:1 Co-Crystal of Hydro­quinone and 3,5-Bis(2-pyridyl)-1,2,4-triazole

Polysulfonylamines. XCI. Ethylammonium Di(benzene­sulfonyl)amide 1,4,7,10,13,16-Hexaoxa­cyclo­octa­decane (1/1/1)

Polysulfonylamines. XCII. 1-Aza-4-azoniabi­cyclo[2.2.2]octane Di(methane­sulfonyl)amidate

Tri­cyclo­hexylphosphoniodi­thioformate

Methyl 3β-Bromine-7α-hy­droxy-5β-cholan-24-oate

1,12-Do­decanediol

[3-(4-Bromo­phenyl)-1-(4-methoxyphenyl)pyrazol-5-yl]aceto­nitrile

(−)-Formoterol, a Selective β₂-Adrenoreceptor Agonist

Three 2,5-Disubstituted 9-Oxabi­cyclo[4.2.1]nonanes. Transannular O-Heterocyclization Products of Cyclo­octa-1,5-diene

Solid Inclusion Compounds of Chiral Roof-Shaped Di­amide Hosts

2'-Hy­droxy-4-N-methylstilbazonium Iodide Methanol Solvate, C₁₄H₁₄NO⁺.I⁻.CH₃OH

Polysulfonylamines. XCVIII. 1,2-Benzenedi­sulfonylamine Aceto­nitrile Solvate (1/1)

A π-Stacked Complex Between 4,4'-Di­methyl-4,4'-bipyridinium Bis(hexa­fluorophosphate) and 1,5-Bis[(hydroxyeth­oxy)eth­oxy]naphthalene

L-Threonine at 12 K

Pyridinium Tri­fluoro­acetate: Spoked Columns of Hydrogen-Bonded Cyclic Dimers

1-Cyano-2-p-bromo­phenylazulene and 2-Azulenylmethyl 2-Anthraquinoate

Tris(1-phenacyl-2-pyridone) Hydroxonium Tetra­fluoroborate, a Hydrogen-Bonded Complex

(−)-2-Azabi­cyclo[2.2.1]hept-5-en-3-one (Lactam)

N-Methyl- and N-Ethylbenzhydrylamine Hydrochloride

endo-1,4,4-Tri­bromo-3-methyltri­cyclo[5.2.1.0^2,6]dec-8-ene-5,10-dione 10-Ethylene Acetal

Spirapril Hydrochloride Hydrate

Methyl 1-Benzyl-3-cyclo­hexyl-2-oxopyrrolidine-2-carboxylate

3-De­oxy-D-fructose

α,α-Di­fluoro-β-lactone and its Non-Fluorinated Analog

2-Acetyl-3-(5-cyano-2-furyl)propene­nitrile

Organo­phosphorus Insecticides. 18. Famphur: O,O-Di­methyl O-[p-(N,N-Di­methylsulfamoyl)phenyl] Phosphoro­thioate

2,4-Di­nitro-N,N-methylphenylaniline

α-Phase p-Di­chloro­benzene at 293K

1,1,1-Tri­fluoro-3-phenyl-2-butyl p-Nitrobenzoate

The Chiral Selector N-(2'-S-Hydroxypropyl)-N,N'-bis­(3,5-di­chloro­benzoyl)-1R,2R-di­amino­cyclo­hexane

Two Tosylated 1,2-O-Iso­propyl­idene-α-D-xylo­furanoses

(5R/5S)-2,5-Di­phenyl-7-[trans-(1R/1S,2S/2R)-2-phenylcyclo­hexyl­oxy]-2,3,5,8-tetra­hydro-1H-1,2,4-triazolo[1,2-a]pyridazine-1,3-dione–Water (1/1): a Face-Selective Diels–Alder Reaction of 2-Alk­oxy-1,3-butadiene

Cyclopropanation of a β-Himachalene Monoepoxide Derivative

3,3-Di­chloro-4-(4-chloro­phenyl)-1-phenylazetidin-2-one

Di­methyl (±)-(1S*,2R*,3S*)-[3-phenyl-1-(N-phenylcarbamoyl­oxy)-2,3-epoxypropyl]phosphonate

The Khellin Quinone

1,3-Bis[bis­(di­methylamino)]-N-methyldiborylamine

Di­phenyl (−)-(R)-1-[(S)-Isoleucyl]pyrrolidine-2-phosphonate Hydrochloride

L-Proline Monohydrate at 100 K

An Extended Imide Containing Two Methylene Meldrum's Acid Units

1,3-Di(eth­oxy-eth­oxy-meth­oxy)calix[4]arene

Oxa-thia-spiro-decene Derivatives

cis-anti-cis-Tri­cyclo[6.4.0.0^2,7]do­decane-3,12-dione and cis-anti-cis-Tri­cyclo[6.4.0.0^2,7]do­decane-3,9-dione

6-Hy­droxy-5,7-di­meth­oxy-4-methylcoumarin

N¹,N²-Di­phenylacetamidine

(3aR,7aS)-N-Tri­phenylmethyl-1,2,3,3a,5,6,7,7a-octa­hydro­pyrano[3,2-b]pyrrol-2-one

(S)-3-(O^γ-Methyl-N^α-tri­phenylmethylglutamyl)benzotriazole 1-Oxide

Bis(4-methoxyphenylsulfonyl)methane: a Three-Dimensional Network Generated by Short C—H⋯O Hydrogen Bonds

Pairwise-Interwoven R⁶₆(48) Hexagonal Nets in the Hydrogen-Bonded Structure of Hexa­methylene­tetramine–1,1,1-Tris(4-hydroxyphenyl)ethane (1/1)

2-(2-Ethoxycarbonyl-1,4-benzodioxan-7-yl)-4H-1-benzo­pyran-4-one

8-Hydroxyquinoline-O-sulfuric Acid and its Monohydrate

5,8-Di­methoxynaphthalene-1,6-di­carboxylic Acid

Hydrogen Bonding and Ring Asymmetry in (±)-cis-2-Phenylcyclo­propane­carboxylic Acid

1,4,5,8-Naphthalene­tetra­carboxylic Acid Cyclic 1,8-Anhydride Bis(di­methyl sulfoxide) Solvate and 1,4,5,8-Naphthalene­tetra­carboxylic 1,8:4,5-Dianhydride

(5aS,7S)-7-Isopropenyl-3-methyl-5a,6,8,9-tetra­hydro-1H,7H-pyrano[4,3-b][1]benzo­pyran-1-one

2-Hy­droxy-5,5-di­methylcyclohex-2-en-1-one

Novel Products from the Rearrangement of Some [n.3.1]Propellanes

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