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Figure 4
(a) Unit-cell length a (top), b (bottom) and c (middle), (b) cell angle β and (c) cell volume V, all as a function of temperature during cooling from 290 to 110 K at a cooling rate of 120 K h−1. Each cell determination is based on a post-refinement (Schreurs, 2008BB20) of 147–150 individual reflections (a = 13.539 + 2.97 × 10 −3 T, b = 5.397 + 0.24 × 10 −3 T, c = 10.879 + 0.29 × 10 −3 T, V = 789.57 + 0.134 T).

Journal logoSTRUCTURAL
CHEMISTRY
ISSN: 2053-2296
Volume 65| Part 2| January 2009| Pages m69-m74
doi:10.1107/S0108270108043242
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