view article
Figure 4
(a) The powder X-ray diffraction patterns of complex (I)[link] and (b) the N2 and CO2 adsorption isotherm (273 K) of (I)[link]. Key: square and triangle curves represent N2 and CO2 adsorption respectively, filled shapes represent adsorption and open shapes represent desorption. In (a), `activated' is the pattern from the crystal sample by heating under a vacuum pretreatment at an optimized temperature of 413 K for 20 h, `simulated' is the pattern from the CIF produced by Mercury (Macrae et al., 2008BB20) and `as synthesized' is the pattern from the synthesized crystal.

Journal logoSTRUCTURAL
CHEMISTRY
ISSN: 2053-2296
Volume 68| Part 8| July 2012| Pages m219-m222
doi:10.1107/S0108270112030582
Follow Acta Cryst. C
Sign up for e-alerts
E-alerts
Follow Acta Cryst. on Twitter
Twitter
Follow us on facebook
Facebook
Sign up for RSS feeds
RSS