Acta Cryst. (2002). E58, m313-m315  [ doi:10.1107/S1600536802009273 ]

Tetraethylammonium dichloro[4,5-dichloro-1,2-bis(2-pyridine-2-carboxamido)benzene]ferrate(III), [Et₄N][(bpc)FeCl₂]

S. J. Lee, J. Y. Lee, H. W. Yang, C. Kim, W. Nam and Y. Kim

Online 31 May 2002

Key indicators

• Single-crystal X-ray study
• T = 298 K
• Mean (C-C) = 0.012 Å
• R factor = 0.044
• wR factor = 0.102
• Data-to-parameter ratio = 8.3

checkCIF results

No syntax errors found

ADDSYM reports no extra symmetry

General Notes



REFLT_03                                                                        
         From the CIF: _diffrn_reflns_theta_max           25.96                 
         From the CIF: _reflns_number_total               2905                  
         Count of symmetry unique reflns         2905                           
         Completeness (_total/calc)            100.00%                          
         TEST3: Check Friedels for noncentro structure                          
         Estimate of Friedel pairs measured         0                           
         Fraction of Friedel pairs measured     0.000                           
         Are heavy atom types Z>Si present          yes                         
          WARNING: Large fraction of Friedel related reflns may                 
                   be needed to determine absolute structure                    

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