Acta Crystallographica Section E
Acta Crystallographica
Section E CRYSTALLOGRAPHIC COMMUNICATIONS

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CRYSTALLOGRAPHIC
COMMUNICATIONS

Volume 58| Part 6

ISSN: 2056-9890

June 2002 issue

Highlighted illustration

Cover illustration: The combination of a sterically generated twist between the two halves of the molecule and standard centrosymmetric pairs of hydrogen bonds for carboxylic acid groups generate a supramolecular assembly of three interpenetrating corrugated sheets for biphenyl-3,3',5,5'-tetracarboxylic acid. See Coles, Holmes, Hursthouse & Price [Acta Cryst. E58, o626-o628].

inorganic compounds

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Ammonium zinc hydrogenphosphite hydrate, (NH₄)₂Zn₅(HPO₃)₆·4H₂O

L. E. Gordon and W. T. A. Harrison

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(NH₄)(Zn,Ga)₂(PO₄)₂, an open-framework structure

M. Mrak, U. Kolitsch, V. Kaučič and E. Tillmanns

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Barium cobalt chloride selenite, Ba₂CoCl₂(SeO₃)₂

M. G. Johnston and W. T. A. Harrison

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Barium palladium selenostannate perselenostannate diselenide, Ba₈Pd(SnSe₄)_3.75(SnSe₅)_0.25(Se₂)

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metal-organic compounds

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(4-tert-Butyl-2-methylthiosemicarbazido)(O-methyldithiophosphato)palladium(II)

M. Janča, J. Taraba and J. Příhoda

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μ-Guanidinido-bis[(terpyridine)platinum(II)] tris(hexafluorophosphate) acetonitrile solvate

M. Kato, A. Toshikawa and S. Kishi

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{[μ-Bis(salicylidene)-1,3-propanediaminato]bis(3,5-dimethylpyridine)nickel(II)}dibromozinc(II)

D. Ülkü, F. B. Kaynak and O. Atakol

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Guanylurea vanadium arsenate

C. A. Bremner and W. T. A. Harrison

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Bis(2-carboethoxyethyl)diiodotin at 120 K

R. A. Howie and S. M. S. V. Wardell

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Dichlorobis(thiourea)cobalt(II) di(4,5-diazafluoren-9-one)

Z.-Y. Wu, D.-J. Xu, J.-Y. Wu and M. Y. Chiang

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Di-μ-hypophosphito-bis[(2,2′-bipyridine)copper(II)] nitrate

G. L. Breneman, M. Fields and O. J. Parker

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Iron methylxanthate

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Chloro(η⁵-cyclopentadienyl){[η⁵:η¹-2-(p-tolylsulfonamido)ethyl]cyclopentadienyl}titanium

C. Lensink and G. J. Gainsford

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Octahedral arrangement of trans-bis(diphenylpropanedionato)bis(o-phenylenediamino)zinc(II)

P. Ovalle-Marroquín, J. Gómez-Lara and S. Hernández-Ortega

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Bis(1,1-dimethylbiguanido)nickel(II)

M. Zhu, L. Lu, P. Yang and X. Jin

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A palladium(0) complex of dibenzylideneacetone and a chelating diphosphine

M. K. Retbøll, E. Wenger and A. C. Willis

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Polymeric di-n-butyl(glutarato)tin(IV)

A. R. Ramirez, M. Parvez, V. U. Ahmad, J. Hussain and H. Hussain

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Triethylammonium (3-carboxyacrylato)dichlorodimethyltin(IV)

B. D. Chandler, M. Parvez, V. U. Ahmad, J. Hussain, H. Hussain and M. Zubair

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Triaquatris(2,6-dinitrophenolato)neodymium(III)

H. R. Suh, H. S. Suh, S. S. Yun, E. K. Lee and S. K. Kang

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Aquaoxobis(quinoline-2-carboxylato-N,O)vanadium(IV) ethanol hemisolvate

N. Okabe and Y. Muranishi

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Sodium p-nitrophenolate tetrahydrate

S. Brahadeeswaran, H. L. Bhat, J. N. Sherwood and R. M. Vrcelj

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catena-Poly[[[1,4-bis(4-pyridyl)-2,3-diaza-1,3-butadiene]silver(I)] nitrate]

Y.-J. Shi, Y.-Z. Li, W.-J. Tong, X.-T. Chen and X.-Z. You

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Dichloro{N-[2-(η⁵-indenyl)ethyl]-p-tolylsulfonamido-κN}titanium

C. Lensink and G. J. Gainsford

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A molecular pair having two quadruply bonded dimolybdenum units linked by a terephthalate dianion

F. A. Cotton, J. P. Donahue, C. Lin, C. A. Murillo and J. Rockwell

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Hexameric isopropyloxotin acetate chloroform tetrasolvate

F. S. Kuan, D. Dakternieks and E. R. T. Tiekink

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A seven-coordinate pyridine-2,6-dicarboxylate-bridged cadmium(II) complex, at 110 K

M. Ranjbar, H. Aghabozorg and A. Moghimi

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catena-Poly[[cadmium(II)]-μ-β-alanine-di-μ-chloro]

M. Subha Nandhini, R. V. Krishnakumar, K. Sivakumar and S. Natarajan

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A solution phase catalyst for an enantioselective Diels–Alder reaction

C. M. Reynoso-Paz, M. M. Olmstead, M. J. Kurth and N. E. Schore

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Tetraethylammonium dichloro[4,5-dichloro-1,2-bis(2-pyridine-2-carboxamido)benzene]ferrate(III), [Et₄N][(bpc)FeCl₂]

S. J. Lee, J. Y. Lee, H. W. Yang, C. Kim, W. Nam and Y. Kim

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organic compounds

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N,N-Bis(trifluoromethylsulfonyl)aniline

J. W. Bats, J. P. Weyrauch and A. S. K. Hashmi

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Dichloromethyl phenyl sulfone

R. Chan-Yu-King, J. Anil, C. Y. Meyers and P. D. Robinson

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N-Phthaloyl-L-alanyl-L-phenylalanine methyl ester

A. R. Hayman and J. Simpson

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(S)-2,2′-Bis(dicyclohexylphosphinoamino)-1,1′-binaphthyl

R. Guo, L. Wang, J. Wu, M. C. K. Choi and Z. Zhou

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2-(Phenanthren-9-ylthiomethylthio)tetrahydropyran at 193 K

J. Kansikas and K. Sipilä

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Hydrogen-bonded molecular chains in (2E)-butane-2,3-dione oxime with Z′ = 3

P. J. Cox and N. M. Foote

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A derivative of diosgenin: (25R)-23-acetyl-3β-bromo-16β-acetoxy-22,26-epoxy-5α-cholest-22-en-6-one

A. Castro-Méndez, J. Sandoval-Ramírez and S. Bernès

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Bergenin monohydrate, a constituent of Hurmiria balsamifera, at 120 K

C. S. Caldas, C. A. De Simone, M. A. Pereira, V. R. S. Malta, R. L. P. Carvalho, T. B. C. Da Silva, A. E. G. Sant'ana and L. M. Conserva

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5-Methyl-2-(4-methylbenzoyloxy)acetophenone

C. Kazak, M. Aygün, C. Kuş, S. Özbey and O. Büyükgüngör

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cis,syn,cis-2,3,4,8,9-Pentachloro-1,5,7,7-tetramethoxytricyclo[4.3.0.0^2,5]nona-3,8-diene

R. Gilardi, D. Tang and P. E. Eaton

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Bis(1-bromo-9-chlorohomocub-9-yl) ether

D. Tang, R. Gilardi and P. E. Eaton

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(3S,4R)-4-(2,5-Dimethoxyphenyl)-8-methoxyisochroman-3-ol

M. Palusiak, M. Małecka, S. J. Grabowski, J. Epsztajn, A. Bieniek and J. A. Kowalska

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The 1:1 complex of hydroquinone and 3-methy-4-nitropyridine 1-oxide

R. Moreno-Fuquen, A. M. Montaño and R. Atencio

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Biphenyl-3,3′,5,5′-tetracarboxylic acid

S. J. Coles, R. Holmes, M. B. Hursthouse and D. J. Price

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3-Ethoxy-7-methoxycarbonyl-4-phenyltricyclo[4.2.1.0^2,5]non-3-ene

M. Schlaf, R. W. Jordan and W. Tam

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2-[(1-Cyano-1-methylethyl)peroxy]-2-methylpropanenitrile

D. Gravestock and M. C. Dovey

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β-Glycine

T. N. Drebushchak, E. V. Boldyreva and E. S. Shutova

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p-Isocyanobenzonitrile

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(1R,2R)-Bis(4-pyridylmethyleneamino)cyclohexane

X.-J. Yuan, Y.-Z. Li, Y.-J. Liu, Y.-Q. Tian and X.-Z. You

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5-Methoxy-2,3-dimethylindole

A. R. Kennedy, J. N. Sherwood and P. A. Slavin

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N-(4-Amino-2-methoxyphenyl)acetamide

M. Robin, J.-P. Galy, A. Kenz and M. Pierrot

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L-Ornithine nitrate

S. Ramaswamy, B. Sridhar, V. Ramakrishnan and R. K. Rajaram

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S-Methyl trans-cis-β-N-(2-hydroxynaphthyl)methylenedithiocarbazate

G. Sethuraman, B. M. Yamin, M. Shamsuddin, A. Usman, I. A. Razak and H.-K. Fun

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Treatment of `twinning' in isopropylcyclohexane

D. R. Allan, P. A. McGregor, L. J. McLachlan, S. Parsons and C. R. Pulham

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N-Benzoyl-N′-(2,6-dimethylphenyl)thiourea

A. Usman, I. A. Razak, S. Satar, M. A. Kadir, B. M. Yamin and H.-K. Fun

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3,3′-Benzylidenebis(4-hydroxy-6-methylcoumarin)

L. Vijayalakshmi, V. Parthasarathi, V. Vora, B. Desai and A. Shah

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Weak C—H⋯O hydrogen bonding and aromatic π–π-stacking interactions in 1-(4-chlorophenyl)propan-1-one

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Benzenesulfonyl(1-hydroxy-1,2-dihydronaphthalen-2-yl)acetonitrile

A. J. Lough, K. Fagnou and M. Lautens

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1,2-Di-2-thienyl-2-hydroxyethanone (2,2′-thenoin)

G. Crundwell, T. Meskill, D. Sayers and K. Kantardjieff

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1,2-Di-3-thienyl-2-hydroxyethanone (3,3′-thenoin)

G. Crundwell, T. Meskill, D. Sayers and K. Kantardjieff

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N-[3-Acetamido-1,3-bis(4-ethylphenyl)butenyl]acetamide

X. Chen, R. Guo and Z. Zhou

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2,6-Dimethyl-3-methylenebicyclo[3.2.1]octane-2,8-diol

S. J. Coles and M. B. Hursthouse

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4,8,9,10-Tetraphenyl-1,3-diazaadamantan-6-one

M. Subha Nandhini, R. V. Krishnakumar, T. Narasimhamurthy, V. Vijayakumar, M. Sundaravadivelu and S. Natarajan

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N-(4-Acetylphenyl)maleamic acid

D. E. Lynch and I. McClenaghan

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3-Cyano-6-(4-methoxyphenyl)-2(1H)-pyridone

D. E. Lynch and I. McClenaghan

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Arjunolic acid

A. Abdul Ajees and K. Balakrishna

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5-Benzoyl-1-cyclohexyl-3-(m-nitrophenyl)-2-phenylpyrrolidine-spiro-4,2′-(6′-methoxy-1′-tetralone)

A. Jeyabharathi, M. N. Ponnuswamy, A. A. Raj, R. Raghunathan and H.-K. Fun

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(E)-1-(4-Carboxyphenylmethylene)-2-tetralone

E. O. Oloo, J. W. Quail, M. P. Padmanilayam and J. R. Dimmock

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1-(4-Carboethoxyphenylmethyl)-2-ethoxynaphthalene

E. O. Oloo, J. W. Quail, M. P. Padmanilayam and J. R. Dimmock

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Spiro[5-carbomethoxy-2-(4-methoxyphenyl)-4-(4-methylphenyl)pyrrolidine-3,3′-chroman-4′-one]

M. N. Nissa, V. Rajakannan, M.-J. Kim, G. Subramaniyan, R. Raghunathan and D. Velmurugan

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2-{[1-(2-Aminophenyl)ethylidene]hydrazino}-5-piperidyl-1,3,4-thiadiazole

A. A. Nassar, J. Valdés-Martínez, S. Hernández-Ortega and D. X. West

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4-Bromophenyl 2,4-dibromophenyl ether

L. Eriksson and J. Hu

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trans-3,6-Dibenzyl-1,2,4,5-tetrazine

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2,3,4,5-Tetrahydro-r-2,c-4-diphenyl-1,5-benzothiazepine

P. Laavanya, K. Panchanatheswaran, M. Muthukumar, R. Jeyaraman and J. A. K. Bauer

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cis-1,2-Dibromo-1,2-diphenylethene–diphenylethyne (2/1)

J. C. Barnes and J. A. Chudek

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Research communications are designed to help authors bring out the science behind their structure determinations. Authors are encouraged to report more than one structure in the same communication and also to include the results of investigations with other techniques. The Research communications format makes Acta E the natural home for structure determinations with interesting science to report.

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