Acta Cryst. (2004). E60, m1757-m1758  [ doi:10.1107/S1600536804027497 ]

(N-Benzoyl-N-phenylhydroxaminato-²O,O')(salicylaldehyde isonicotinoylhydrazonato-³O,N,N')vanadium(IV) hexane hemisolvate

S. Gao, L.-H. Huo, H. Zhao and S. W. Ng

Online 6 November 2004

Key indicators

• Single-crystal X-ray study
• T = 295 K
• Mean (C-C) = 0.005 Å
• R factor = 0.058
• wR factor = 0.141
• Data-to-parameter ratio = 17.3

checkCIF/PLATON results

No syntax errors found




Alert level C
ABSTM02_ALERT_3_C  The ratio of expected to reported Tmax/Tmin(RR') is < 0.90
            Tmin and Tmax reported:      0.725     0.926
            Tmin' and Tmax expected:      0.849     0.925
            RR' =      0.853
            Please check that your absorption correction is appropriate.
PLAT042_ALERT_1_C Calc. and Rep. MoietyFormula Strings Differ ....          ?
PLAT061_ALERT_3_C Tmax/Tmin Range Test RR' too Large .............       0.85       
PLAT068_ALERT_1_C Reported F000 Differs from Calcd (or Missing)...          ?
PLAT152_ALERT_1_C Supplied and Calc Volume s.u. Inconsistent .....          ?
PLAT232_ALERT_2_C Hirshfeld Test Diff (M-X)  V1     -   N1      ..       5.35 su    
PLAT420_ALERT_2_C D-H Without Acceptor       N2     -   H2N    ...          ?       
PLAT710_ALERT_4_C Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... #         11     
            O5  -V1  -O3  -C14     5.00  0.80   1.555   1.555   1.555   1.555   

   0 ALERT level A = In general: serious problem
   0 ALERT level B = Potentially serious problem
   8 ALERT level C = Check and explain
   0 ALERT level G = General alerts; check

   3 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   2 ALERT type 2 Indicator that the structure model may be wrong or deficient
   2 ALERT type 3 Indicator that the structure quality may be low
   1 ALERT type 4 Improvement, methodology, query or suggestion

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