Acta Cryst. (2008). E64, m608  [ doi:10.1107/S1600536808004881 ]

Decacarbonyl-1³C,2³C,3⁴C--hydrido-1:2²H:H-(-quinoline-2-thiolato-1:2²S:S)diosmium(I)osmium(0)(3 Os-Os)

Y. Sun, X.-B. Li and B.-W. Sun

Online 2 April 2008

Key indicators

• Single-crystal X-ray study
• T = 223 K
• Mean (C-C) = 0.009 Å
• R factor = 0.024
• wR factor = 0.052
• Data-to-parameter ratio = 14.3

checkCIF/PLATON results

No syntax errors found




Alert level C
PLAT222_ALERT_3_C Large Non-Solvent    H     Ueq(max)/Ueq(min) ...       3.33 Ratio
PLAT342_ALERT_3_C Low Bond Precision on C-C Bonds (x 1000) Ang ...          9      

Alert level G
PLAT860_ALERT_3_G Note: Number of Least-Squares Restraints .......          1      

   0 ALERT level A = In general: serious problem
   0 ALERT level B = Potentially serious problem
   2 ALERT level C = Check and explain
   1 ALERT level G = General alerts; check

   0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   0 ALERT type 2 Indicator that the structure model may be wrong or deficient
   3 ALERT type 3 Indicator that the structure quality may be low
   0 ALERT type 4 Improvement, methodology, query or suggestion
   0 ALERT type 5 Informative message, check

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