Acta Cryst. (2009). E65, m793  [ doi:10.1107/S1600536809022405 ]

{Bis[2-(diphenylphosphino)ethyl]phenylphosphine-³P,P',P''}chloridoplatinium(II) hexafluoridophosphate

S. A. Heston, B. C. Noll and M. L. Helm

Online 20 June 2009

Key indicators

• Single-crystal X-ray study
• T = 298 K
• Mean (C-C) = 0.006 Å
• Disorder in solvent or counterion
• R factor = 0.020
• wR factor = 0.049
• Data-to-parameter ratio = 13.6

checkCIF/PLATON results

No syntax errors found




Alert level C
PLAT214_ALERT_2_C Atom F6      (Anion/Solvent) ADP max/min Ratio         4.30 prola
PLAT241_ALERT_2_C Check High      Ueq as Compared to Neighbors for         C3     
PLAT242_ALERT_2_C Check Low       Ueq as Compared to Neighbors for         C1     
PLAT244_ALERT_4_C Low   'Solvent' Ueq as Compared to Neighbours of         P4     

Alert level G
PLAT860_ALERT_3_G Note: Number of Least-Squares Restraints .......        204      
PLAT302_ALERT_4_G Note Anion/Solvent Disorder ....................      36.00 Perc.

   0 ALERT level A = In general: serious problem
   0 ALERT level B = Potentially serious problem
   4 ALERT level C = Check and explain
   2 ALERT level G = General alerts; check

   0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   3 ALERT type 2 Indicator that the structure model may be wrong or deficient
   1 ALERT type 3 Indicator that the structure quality may be low
   2 ALERT type 4 Improvement, methodology, query or suggestion
   0 ALERT type 5 Informative message, check

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