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Acta Cryst. (2012). E68, m1346
[ doi:10.1107/S1600536812042110 ]

[Hydridotris(pyrazol-1-yl-[kappa]N2)borato]bis(methylamino-[kappa]N)(triphenylphosphine-[kappa]P)ruthenium(II) chloride dichloromethane solvate monohydrate

Y.-D. Lin, C.-P. Chang, Q.-S. Huang and Y.-H. Lo


Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level C PLAT026_ALERT_3_C Ratio Observed / Unique Reflections too Low .... 47 Perc. PLAT243_ALERT_4_C High 'Solvent' Ueq as Compared to Neighbors of C30 PLAT342_ALERT_3_C Low Bond Precision on C-C Bonds ............... 0.0125 Ang PLAT420_ALERT_2_C D-H Without Acceptor N7 - H7A ... ? PLAT420_ALERT_2_C D-H Without Acceptor N8 - H8B ... ? PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 9.912 PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.595 43 PLAT973_ALERT_2_C Large Calcd. Positive Residual Density on Ru1 1.04 eA-3
Alert level G PLAT005_ALERT_5_G No _iucr_refine_instructions_details in CIF .... ? PLAT007_ALERT_5_G Note: Number of Unrefined D-H Atoms ............ 6 PLAT042_ALERT_1_G Calc. and Reported MoietyFormula Strings Differ ?
0 ALERT level A = Most likely a serious problem - resolve or explain 0 ALERT level B = A potentially serious problem, consider carefully 8 ALERT level C = Check. Ensure it is not caused by an omission or oversight 3 ALERT level G = General information/check it is not something unexpected 1 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 3 ALERT type 2 Indicator that the structure model may be wrong or deficient 4 ALERT type 3 Indicator that the structure quality may be low 1 ALERT type 4 Improvement, methodology, query or suggestion 2 ALERT type 5 Informative message, check

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