[Open access]

[Contents scheme]

Acta Cryst. (2012). E68, m1354-m1355
[ doi:10.1107/S1600536812042286 ]

Bis(diphenyl-p-tolylphosphane-[kappa]P)(2-hydroxy-3,5,7-bromocyclohepta-2,4,6-trienonato-[kappa]2O,O')copper(I)

N. I. Barnard and T. N. Hill


Key indicators

checkCIF/PLATON results

No syntax errors found



Datablock: I



Alert level B PLAT230_ALERT_2_B Hirshfeld Test Diff for Br2 -- C5 .. 8.0 su
Alert level C PLAT242_ALERT_2_C Check Low Ueq as Compared to Neighbors for C5
Alert level G PLAT005_ALERT_5_G No _iucr_refine_instructions_details in CIF .... ? PLAT083_ALERT_2_G SHELXL Second Parameter in WGHT Unusually Large. 16.66 PLAT380_ALERT_4_G Check Incorrectly? Oriented X(sp2)-Methyl Moiety C137 PLAT912_ALERT_4_G Missing # of FCF Reflections Above STh/L= 0.600 28 PLAT960_ALERT_3_G Number of Intensities with I .LT. - 2*sig(I) ... 2
0 ALERT level A = Most likely a serious problem - resolve or explain 1 ALERT level B = A potentially serious problem, consider carefully 1 ALERT level C = Check. Ensure it is not caused by an omission or oversight 5 ALERT level G = General information/check it is not something unexpected 0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 3 ALERT type 2 Indicator that the structure model may be wrong or deficient 1 ALERT type 3 Indicator that the structure quality may be low 2 ALERT type 4 Improvement, methodology, query or suggestion 1 ALERT type 5 Informative message, check

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