[Open access]

[Contents scheme]

Acta Cryst. (2012). E68, m1330-m1331
[ doi:10.1107/S1600536812040810 ]

trans-Dichloridobis[dicyclohexyl(2,4,6-trimethylphenyl)phosphane-[kappa]P]palladium(II)

I. Buthelezi, H. Chiririwa, H. Ogutu and R. Meijboom


Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level C PLAT029_ALERT_3_C _diffrn_measured_fraction_theta_full Low ....... 0.979 PLAT342_ALERT_3_C Low Bond Precision on C-C Bonds ............... 0.0081 Ang PLAT905_ALERT_3_C Negative K value in the Analysis of Variance ... -0.580 PLAT910_ALERT_3_C Missing # of FCF Reflections Below Th(Min) ..... 1 PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.600 32 PLAT973_ALERT_2_C Large Calcd. Positive Residual Density on Pd1 1.39 eA-3
Alert level G PLAT005_ALERT_5_G No _iucr_refine_instructions_details in CIF .... ? PLAT153_ALERT_1_G The su's on the Cell Axes are Equal .......... 0.00500 Ang. PLAT154_ALERT_1_G The su's on the Cell Angles are Equal .......... 0.00500 Deg. PLAT343_ALERT_2_G Check sp? Angle Range in Main Residue for .. C1 PLAT343_ALERT_2_G Check sp? Angle Range in Main Residue for .. C16 PLAT793_ALERT_4_G The Model has Chirality at P1 (Verify) .... S PLAT912_ALERT_4_G Missing # of FCF Reflections Above STh/L= 0.600 74 PLAT960_ALERT_3_G Number of Intensities with I .LT. - 2*sig(I) ... 4
0 ALERT level A = Most likely a serious problem - resolve or explain 0 ALERT level B = A potentially serious problem, consider carefully 6 ALERT level C = Check. Ensure it is not caused by an omission or oversight 8 ALERT level G = General information/check it is not something unexpected 2 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 3 ALERT type 2 Indicator that the structure model may be wrong or deficient 6 ALERT type 3 Indicator that the structure quality may be low 2 ALERT type 4 Improvement, methodology, query or suggestion 1 ALERT type 5 Informative message, check

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