[Open access]

[Contents scheme]

Acta Cryst. (2013). E69, m77-m78
[ doi:10.1107/S1600536812052002 ]

cis-Bis(2,2'-bipyridine-[kappa]2N,N')bis(pyridin-4-amine-[kappa]N1)ruthenium(II) bis(hexafluoridophosphate) acetonitrile monosolvate

M. R. Camilo, F. T. Martins, V. R. S. Malta, J. Ellena and R. M. Carlos


Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level B PLAT910_ALERT_3_B Missing # of FCF Reflections Below Th(Min) ..... 12 PLAT934_ALERT_3_B Number of (Iobs-Icalc)/SigmaW .gt. 10 Outliers . 1
Alert level C PLAT244_ALERT_4_C Low 'Solvent' Ueq as Compared to Neighbors of P1 PLAT244_ALERT_4_C Low 'Solvent' Ueq as Compared to Neighbors of P1A PLAT244_ALERT_4_C Low 'Solvent' Ueq as Compared to Neighbors of C1S PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 3.311 PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.600 2 PLAT913_ALERT_3_C Missing # of Very Strong Reflections in FCF .... 1
Alert level G PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF ? PLAT007_ALERT_5_G Note: Number of Unrefined D-H Atoms ............ 4 PLAT180_ALERT_4_G Check Cell Rounding: # of Values Ending with 0 = 3 PLAT232_ALERT_2_G Hirshfeld Test Diff (M-X) Ru -- N2 .. 5.1 su PLAT720_ALERT_4_G Number of Unusual/Non-Standard Labels .......... 3 PLAT912_ALERT_4_G Missing # of FCF Reflections Above STh/L= 0.600 279
0 ALERT level A = Most likely a serious problem - resolve or explain 2 ALERT level B = A potentially serious problem, consider carefully 6 ALERT level C = Check. Ensure it is not caused by an omission or oversight 6 ALERT level G = General information/check it is not something unexpected 0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 1 ALERT type 2 Indicator that the structure model may be wrong or deficient 5 ALERT type 3 Indicator that the structure quality may be low 6 ALERT type 4 Improvement, methodology, query or suggestion 2 ALERT type 5 Informative message, check

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