[Open access]

[Contents scheme]

Acta Cryst. (2013). E69, o169-o170
[ doi:10.1107/S1600536812051458 ]

3-({4-[(2-Methylbenzylidene)amino]-5-sulfanylidene-1H-1,2,4-triazol-3-yl}methyl)-1,3-benzoxazol-2(3H)-one

A. Aydin, N. Hekimoglu, M. Akkurt, T. Önkol, S. U. Çiçekli and O. Büyükgüngör


Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level C PLAT334_ALERT_2_C Small Average Benzene C-C Dist. C1 -C6 1.37 Ang. PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 9.593 PLAT910_ALERT_3_C Missing # of FCF Reflections Below Th(Min) ..... 1 PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.600 50
Alert level G PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF ? PLAT007_ALERT_5_G Note: Number of Unrefined D-H Atoms ............ 1 PLAT063_ALERT_4_G Crystal Size Likely too Large for Beam Size .... 0.62 mm PLAT912_ALERT_4_G Missing # of FCF Reflections Above STh/L= 0.600 22
0 ALERT level A = Most likely a serious problem - resolve or explain 0 ALERT level B = A potentially serious problem, consider carefully 4 ALERT level C = Check. Ensure it is not caused by an omission or oversight 4 ALERT level G = General information/check it is not something unexpected 0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 1 ALERT type 2 Indicator that the structure model may be wrong or deficient 3 ALERT type 3 Indicator that the structure quality may be low 2 ALERT type 4 Improvement, methodology, query or suggestion 2 ALERT type 5 Informative message, check
checkCIF publication errors
Alert level A PUBL024_ALERT_1_A The number of authors is greater than 5. Please specify the role of each of the co-authors for your paper.
Author Response: Each of the authors has been involved in this study: A. Aydin - structure solution and refinement, N. Hekimoglu - publication stage, M. Akkurt - theoretical approach, T. Onkol - synthesis and biologigal activitity, S. Urlu-Cicekli - synthesis, O. Buyukgungor - data collection.

1 ALERT level A = Data missing that is essential or data in wrong format 0 ALERT level G = General alerts. Data that may be required is missing

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