(IUCr) Crystallography Journals Online checkcif report

[Contents scheme]

Acta Cryst. (2013). E69, o167-o168
[ doi:10.1107/S1600536812051537 ]

(Pyridin-4-yl)methyl N'-(3-phenylallylidene)hydrazinecarbodithioate

M. L. Low, T. B. S. A. Ravoof, M. I. M. Tahir, K. A. Crouse and E. R. T. Tiekink

Key indicators

Single-crystal X-ray study
T = 100 K
Mean (C-C) = 0.003 Å
R factor = 0.042
wR factor = 0.115
Data-to-parameter ratio = 15.1

checkCIF/PLATON results

No syntax errors found




Alert level C
PLAT029_ALERT_3_C _diffrn_measured_fraction_theta_full Low .......      0.971      
PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L=  0.600          5      

Alert level G
PLAT002_ALERT_2_G Number of Distance or Angle Restraints on AtSite          2      
PLAT005_ALERT_5_G No _iucr_refine_instructions_details  in the CIF          ?
PLAT860_ALERT_3_G Note: Number of Least-Squares Restraints .......          1      
PLAT912_ALERT_4_G Missing # of FCF Reflections Above STh/L=  0.600         81      

   0 ALERT level A = Most likely a serious problem - resolve or explain
   0 ALERT level B = A potentially serious problem, consider carefully
   2 ALERT level C = Check. Ensure it is not caused by an omission or oversight
   4 ALERT level G = General information/check it is not something unexpected

   0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   1 ALERT type 2 Indicator that the structure model may be wrong or deficient
   3 ALERT type 3 Indicator that the structure quality may be low
   1 ALERT type 4 Improvement, methodology, query or suggestion
   1 ALERT type 5 Informative message, check