[Open access]

[Contents scheme]

Acta Cryst. (2013). E69, m339
[ doi:10.1107/S1600536813013470 ]

Bis[[mu]-1,3-bis(diphenylphosphanyl)propane-[kappa]2P:P']digold(I) tetrachloridonickelate(II) diethyl ether monosolvate

A. Igashira-Kamiyama, T. Itai, Y. Arai and T. Konno


Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level B PLAT910_ALERT_3_B Missing # of FCF Reflections Below Th(Min) ..... 19 PLAT934_ALERT_3_B Number of (Iobs-Icalc)/SigmaW > 10 Outliers .... 3 PLAT973_ALERT_2_B Large Calcd. Positive Residual Density on Au2 1.68 eA-3 PLAT973_ALERT_2_B Large Calcd. Positive Residual Density on Au1 1.56 eA-3
Alert level C PLAT244_ALERT_4_C Low 'Solvent' Ueq as Compared to Neighbors of Ni1 PLAT244_ALERT_4_C Low 'Solvent' Ueq as Compared to Neighbors of O1 PLAT342_ALERT_3_C Low Bond Precision on C-C Bonds ............... 0.0087 Ang PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 8.891 PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 2.438 PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.600 6 PLAT972_ALERT_2_C Large Calcd. Non-Metal Negative Residual Density -1.58 eA-3
Alert level G PLAT002_ALERT_2_G Number of Distance or Angle Restraints on AtSite 12 PLAT003_ALERT_2_G Number of Uiso or Uij Restrained non-H Atoms ... 12 PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF ? PLAT083_ALERT_2_G SHELXL Second Parameter in WGHT Unusually Large. 5.06 PLAT128_ALERT_4_G Note: Alternate Setting of Space-group P21/c . P21/n PLAT301_ALERT_3_G Note: Main Residue Disorder ................... 10 % PLAT860_ALERT_3_G Note: Number of Least-Squares Restraints ....... 78 PLAT912_ALERT_4_G Missing # of FCF Reflections Above STh/L= 0.600 15
0 ALERT level A = Most likely a serious problem - resolve or explain 4 ALERT level B = A potentially serious problem, consider carefully 7 ALERT level C = Check. Ensure it is not caused by an omission or oversight 8 ALERT level G = General information/check it is not something unexpected 0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 6 ALERT type 2 Indicator that the structure model may be wrong or deficient 8 ALERT type 3 Indicator that the structure quality may be low 4 ALERT type 4 Improvement, methodology, query or suggestion 1 ALERT type 5 Informative message, check

Copyright © International Union of Crystallography
IUCr Webmaster