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Figure 3
(a) The cell parameters of samples A and B from synchrotron single-crystal X-ray diffraction (SXRD) and conventional powder X-ray diffraction (PXRD). (b) The (204) reflection plotted as a function of temperature collected with a conventional X-ray source (sample B). (c) A high-resolution synchrotron PXRD pattern showing asymmetries at 550 K (sample B).

IUCrJ
Volume 3| Part 5| September 2016| Pages 377-388
ISSN: 2052-2525
doi:10.1107/S2052252516012707