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Figure 1
Fe K-edge XANES data measured from a 0.1 M Fe(II)Cl2 aqueous solution sample, upon (a) heating and (b) cooling, using a bending-magnet beamline of the Cornell High Energy Synchrotron Source (CHESS). The thermal history of the sample is illustrated in (c); the XANES measured from a 0.1 M Fe(III)Cl3 aqueous solution sample at 298 K (dashed line) is shown in (a) for comparison. The Fe(II)Cl2 aqueous solution sample was exposed discontinuously to synchrotron radiation for approximately half of the 87 h duration of the experiment (Anderson et al., 2012BB1).

Journal logoJOURNAL OF
SYNCHROTRON
RADIATION
ISSN: 1600-5775
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