X-ray spectroscopy for chemistry in the 2-4 keV energy regime at the XMaS beamline: ionic liquids, Rh and Pd catalysts in gas and liquid environments, and Cl contamination in γ-Al2O3

Thompson, P.B.J.; Nguyen, B.N.; Nicholls, R.; Bourne, R.A.; Brazier, J.B.; Lovelock, K.R.J.; Brown, S.D.; Wermeille, D.; Bikondoa, O.; Lucas, C.A.; Hase, T.P.A.; Newton, M.A.

doi:10.1107/S1600577515016148

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Figure 15
(a) Normalized Cl K-edge XANES for a 5 wt% Pd/Al₂O₃ catalyst derived from a PdCl₂ precursor; and (b) the corresponding Pd L₃-edge spectra. As previously, spectra are shown for the dry (in He) powder catalyst, that made wet by the flowing solvent at RT, and that obtained after heating in situ to 353 K under flowing ethanol–water.

JOURNAL OF
SYNCHROTRON
RADIATION

ISSN: 1600-5775

Volume 22| Part 6| October 2015| Pages 1426-1439

doi:10.1107/S1600577515016148

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