(IUCr) Acta Crystallographica Section B Volume 33, Part 12, December 1977

Stereoisomerism in partial bile pigment structures. The crystal structures of the Z and E isomers of 5'-ethoxycarbonyl-3,4-dihydro-3',4'-dimethyl-5(1H)-2,2'-pyrromethenone and their reaction products with Et₃O⁺BF₄⁻

W. S. Sheldrick, A. Borkenstein, M. Blacha-Puller and A. Gossauer

CCDC references: 1148446; 1149128; 1150801; 1311937

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The crystal and molecular structure of DL-mannitol at –150°C

J. A. Kanters, G. Roelofsen and D. Smits

CCDC references: 1142428; 1142429

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Steroids and related studies. XXXIX. The crystal structure and stereochemistry of 17a-methyl-3β-pyrrolidinyl-17a-aza-D-homo-5-androstene (HS-309)

M. A. Mazid, R. A. Palmer, H. Singh and D. Paul

CCDC reference: 1214316

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The crystal structure of sodium percarbonate: an unusual layered solid

J. M. Adams and R. G. Pritchard

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The crystal structure of guanidinium pyrophosphate monohydrate

J. M. Adams and V. Ramdas

CCDC reference: 1170726

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Electron density distribution in cumulenes: an X-ray study of tetraphenylbutatriene at 20°C and –160°C

Z. Berkovitch-Yellin and L. Leiserowitz

CCDC references: 1275120; 1275121

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Electron density distribution in cumulenes: an X-ray study of the complex allenedicarboxylic acid–acetamide (1:1) at –l50°C

Z. Berkovitch-Yellin, L. Leiserowitz and F. Nader

CCDC reference: 1102255

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The crystal structure of 2'-deoxy-6-thioguanosine monohydrate

G. L. Gartland and C. E. Bugg

CCDC reference: 1145551

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Solid-state phase transition in carbon tetrabromide CBr₄. I. The crystal structure of phase II at room temperature

M. More, F. Baert and J. Lefebvre

CCDC reference: 1131866

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The crystal structure of [1,2,5]thiadiazolo[3,4-g]benzofurazan 1-oxide, C₆H₂N₄O₂S

M. Calleri, L. Bonaccorti and D. Viterbo

CCDC reference: 1277518

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The molecular structure of μ-cyclopentadienyl-μ-bromo-bis(triisopropylphosphine)dipalladium

A. Ducruix and C. Pascard

CCDC reference: 1237951

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Structure cristalline de NaSbBrF₃.H₂O

B. Ducourant, B. Bonnet, R. Fourcade and G. Mascherpa

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Structure moléculaire et cristalline de l'alcalöide crinamine

R. Roques, J. P. Declercq and G. Germain

CCDC reference: 1131670

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Crystal structure and conformation of 3-deaza-4-deoxyuridine

E. Egert, H. J. Lindner, W. Hillen and H. G. Gassen

CCDC reference: 1249279

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The crystal and molecular structure of bis(triphenylphosphine)[2-3-η-(1,4-benzoquinone)]platinum(0)

R. S. Vagg

CCDC reference: 1229348

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The crystal structure of γ-bis(ethylammonium) tetrachloromanganate(II) at 126 K and its phase transition

W. Depmeier

CCDC reference: 1148005

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The crystal and molecular structure of 1,3,4,6-tetra-O-acetyl-2,5-O-methylene-D-mannitol: the solid state conformation of a 1,3-dioxepane ring

T. S. Cameron, R. E. Cordes and T. B. Grindley

CCDC reference: 1102660

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Structure cristalline du fluoroindate de potassium KIn₂F₇

J.-C. Champarnaud-Mesjard and B. Frit

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Distortions in substituted benzene rings: geometric constraints on the distortion of a planar ring

D. Britton

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The crystal structure of synthetic sodium pentaborate monohydrate

S. Menchetti and C. Sabelli

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Refinement of the crystal structure of di-μ-fluoro-hexafluorohexaaquadizirconium(IV), Zr₂F₈(H₂O)₆

F. Gabela, B. Kojić-Prodić, M. Šljukić and Ž. Rużić-Toroš

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Stereochemistry of unsaturated amino sugars. II. The crystal and molecular structures of peracetylated 1,2-dideoxy-D-xylo- and D-ribo-aldopyranoses, C₁₆H₂₁O₉N

V. Rogić, Ž. Rużić-Toroš, B. Kojić-Prodić and N. Pravdić

CCDC references: 1100402; 1100553

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The crystal and molecular structure of piflutixol, a tricyclic neuroleptic drug

P. G. Jones, O. Kennard and A. S. Horn

CCDC reference: 1233239

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Un exemple de délocalisation électronique totale dans l'anneau cyclobutadiénique: structure cristalline et moléculaire de {[(C₂H₅)₄C₄]NiBr₂}₂

G. Guerch, P. Mauret, J. Jaud and J. Galy

CCDC reference: 1148459

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Etude de chromates, molybdates et tungstates hydratés. II. Etude structurale de CaCrO₄.H₂O

O. Bars, J.-Y. Le Marouille and D. Grandjean

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The crystal and molecular structure of cholest-4-en-6-one

L. R. Nassimbeni, J. C. Russell and G. M. L. Cragg

CCDC reference: 1124373

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Structure cristalline du butanedisulfonate-1,4 de cuivre tétrahydraté: Cu[SO₃(CH₂)₄SO₃].4H₂O

F. Charbonnier, R. Faure and H. Loiseleur

CCDC reference: 1116038

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The crystal structure of chlorobis(triphenylphosphine)tris(4-tolyl isocyanide)iron(II) tetrachloroferrate(III)

G. Pelizzi, G. Albertin, E. Bordignon, A. A. Orio and S. Calogero

CCDC reference: 1131923

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The crystal structure of Ag₂BrNO₃

K. Persson and B. Holmberg

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The crystal and molecular structure of tris(thiourea)copper(I) hydrogen-o-phthalate. A monomeric trigonal planar copper(I) complex

M. B. Cingi, A. M. M. Lanfredi, A. Tiripicchio and M. T. Camellini

CCDC reference: 1276136

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The crystal and molecular structure of 2,4,6-tris(2'-pyridinio)-1,3,5-triazine pentachloromanganate(III) chloride monohydrate

G. A. Barclay, R. S. Vagg and E. C. Watton

CCDC reference: 1240890

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The crystal and molecular structure of 25-isosolafloridine hydrochloride

B. M. Gatehouse and A. J. Jozsa

CCDC reference: 1180950

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La structure cristalline et moléculaire du tribenzamide, N(COC₆H₅)₃

A. Caron, C. Riche, C. Pascard-Billy and J.-C. Gramain

CCDC references: 1275646; 1275647

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Structure d'une deuxième variété cristalline du dioxodichlorobis(hexaméthylphosphoramide)molybdène(VI)

B. Viossat, P. Khodadad and N. Rodier

CCDC reference: 1177129

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Deformation electron density of α-glycylglycine at 82 K. I. The neutron diffraction study

Å. Kvick, A. R. Al-Karaghouli and T. F. Koetzle

CCDC reference: 1169399

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Some structures topologically related to cubic perovskite (E2₁), ReO₃ (D0₉) and Cu₃Au (L1₂)

M. O'Keeffe and B. G. Hyde

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A simple refinement of density distributions of bonding electrons. I. A description of the proposed method

E. Hellner

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A simple refinement of density distributions of bonding electrons. II. Bond electron density distribution in diborane

D. Mullen and E. Hellner

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The structure of a 1:1 mixed crystal of L-glutamic acid and L-pyroglutamic acid, C₅H₉NO₄.C₅H₇NO₃.H₂O, and a refinement of the structure of pyroglutamic acid, C₅H₇NO₃

Z. Taira and W. H. Watson

CCDC references: 1206535; 1240748

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Structure cristalline du complexe 4,4',5,5'-tétraéthyltétrathiofulvalène–bis(tétracyanoquinodiméthane), (TETTF)(TCNQ)₂

J. L. Galigné, J. M. Fabre and L. Firal

CCDC reference: 1150465

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The structures of L- and meso-diaminopimelic acid hydrochlorides

S. E. Hull, O. Kennard, H. J. Rogers and M. V. Kelemen

CCDC references: 1204450; 1210406

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The structure and stereochemistry of α- and β-cubebene from the crystal structure of norcubebanone, C₁₄H₂₂O

W. E. Thiessen

CCDC reference: 1217935

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Crystal and molecular structure of the bimetallocarborane complex: tetramethylammonium 2,3-di-η-cyclopentadienyl-2,3-dicobalta-1-carbadodecaborate

V. Šubrtová, A. Línek, C. Novák, V. Petříček and J. Ječný

CCDC reference: 1128077

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Liaison hydrogène et cétoénolisation en série barbiturique à l'état cristallin. II. Structure cristalline par diffraction des neutrons de l'acide diéthyl-1,3-thio-2 barbiturique

J.-P. Bideau, G. Bravic and A. Filhol

CCDC reference: 1139343

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Etude structurale d'un thiospinelle d'étain Fe₂SnS₄

J.-C. Jumas, E. Philippot and M. Maurin

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Structural studies of benzene derivatives. III. The crystal and molecular structure of p-nitrobenzamide

F. Di Rienzo, A. Domenicano and E. F. Serantoni

CCDC reference: 1223500

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The crystal structure of magnesium dimolybdate

K. Stadnicka, J. Haber and R. Kozłowski

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Solid-state phase transition in carbon tetrabromide. II. The crystal structure of phase I

M. More, J. Lefebvre and R. Fouret

CCDC reference: 1131867

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4,5-Dichloro-l,3,6,8-tetrafluoro-2,7-naphthyridine

D. M. W. van den Ham and G. J. van Hummel

CCDC reference: 1124263

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Céphapyrine

J. P. Declercq, G. Germain, C. Moreaux and M. Van Meerssche

CCDC reference: 1123204

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Bis(N-méthyl N-phénylamino)-3,3 propadiène thione-1

M. Van Meerssche, G. Germain, J. P. Declercq, H. G. Viehe and M. Parmentier

CCDC reference: 1213758

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Bis(N-méthyl N-phénylamino)-4,4 phényl-1 butatriènecarbonitrile-1

M. Van Meerssche, G. Germain, J. P. Declercq, H. G. Viehe and M. Parmentier

CCDC reference: 1103237

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Acide mercapto-2 pyridinecarboxylique-4

J. P. Declercq, A. Schanck, G. Germain, J. M. Dereppe and M. Van Meerssche

CCDC reference: 1214243

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Acide mercapto-2 pyridinecarboxylique-6 hémihydraté

G. Germain, J. P. Declercq, A. Schanck, J. M. Dereppe and M. Van Meerssche

CCDC reference: 1211288

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Diméthylamino-4 (diméthylamino)méthylène-5 phénylimino-2 oxazoline. Un produit inattendu de réaction d'un isocyanate avec une ynamine-amidine

J. P. Declercq, G. Germain, M. Van Meerssche, B. Caillaux and H. G. Viehe

CCDC reference: 1209310

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Méthoxycarbonyl-7a diaza-1,2 dibenzo-4,5,6,7 bicyclo[4.3.0]nonène-1

F. Chentli-Benchikha, J. P. Declercq, G. Germain and M. Van Meerssche

CCDC reference: 1210401

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Bis(N-acetylglycinato)-1,10-phenanthrolinecopper(II)

L. P. Battaglia, A. B. Corradi, G. Marcotrigiano and G. C. Pellacani

CCDC reference: 1100681

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2-Phenylsparteine N(16)-oxide monoperchlorate

H. Małuszyńska and Y. Okaya

CCDC reference: 1238318

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Dihydroxy-5,6 canrénone

E. Surcouf

CCDC reference: 1139956

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10-Methyl-2,2'-bis(trifluoromethyl)-7,10'-biphenothiazine

K. Go, G. Kartha and K. Nagarajan

CCDC reference: 1214710

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Sulfure d'europium et d'étain Eu₃Sn₂S₇

S. Jaulmes and M. Julien-Pouzol

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Bis(m-chlorophenyl)acetylene

A. A. Espiritu and J. G. White

CCDC reference: 1142561

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Cyclo-L-leucyl-L-histidyl monohydrate

I. Tanaka, T. Iwata, N. Takahashi, T. Ashida and M. Tanihara

CCDC reference: 1127149

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Triple-layered [2.2]metacyclophane, methylated derivative of the uu isomer

F. Hama, Y. Kai, N. Yasuoka and N. Kasal

CCDC reference: 1210984

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(+)-O-Methyl-α-phenylphosphinylpropionic acid

Z. Gałdecki and M. L. Głowka

CCDC reference: 1213927

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S,S-Dimethyl-N-(2-oxo-1-indolinyl)sulfoximide

M. D. Cabezuelo, C. Foces-Foces, F. H. Cano and S. García-Blanco

CCDC reference: 1215339

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2-Phenylcyclopropane-1-spiro-4'-(2'-benzylthio-4',5'-dihydro-6'H-1',3'-thiazine)-5'-spiro-2''-oxirane (CTO)

M. L. Martínez, F. H. Cano and S. García-Blanco

CCDC reference: 1130874

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η⁴-(1-endo-Ethyl)cyclopentadiene-η⁵-cyclopentadienyl(triethylphosphine)chloromolybdenum(II)

E. Cannillo and K. Prout

CCDC reference: 1131019

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7,7,9,9-Tetramethyl-8-thiosulphinyliminothio-1,4-dioxa-8-azaspiro[4,5]decane

C. Tamura, K. Aiba, S. Sato, T. Hata, S. Morimura and T. Yoshioka

CCDC reference: 1275884

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The ethyl carbonate of 1-isoquinolyl(phenyl)methanol

E. Skrzypczak-Jankun and Z. Kałuski

CCDC reference: 1180823

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1-(2-Pyridyl)-5-methylimidazole

D. C. Mente, R. J. Sundberg and R. F. Bryan

CCDC reference: 1240503

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p-Fluorobenzonitrile

D. Britton and W. B. Gleason

CCDC reference: 1232148

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2,2,8-Trimethyltricyclo[6.2.2.0^1,6]dodec-5-ene-9,10-dicarboxylic anhydride

P. Murray-Rust and J. Murray-Rust

CCDC reference: 1272421

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Humulene triepoxide

P. Murray-Rust and J. Murray-Rust

CCDC reference: 1178651

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A neutron diffraction study of lanthanum magnesium nitrate La₂-Mg₃(NO₃)₁₂.24H₂O

M. R. Anderson, G. T. Jenkin and J. W. White

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Ethylenediamine citrate

N. Gavrushenko, H. L. Carrell, W. C. Stallings and J. P. Glusker

CCDC reference: 1126247

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8,9,10,11,11a,11b,12,13-Octahydro-6H,7aH-benzo[5,6][1,3]oxazino[3,4-a]quinoline

A. Griffiths

CCDC reference: 1225910

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Bis(1,2-diphenyl-1,2-ethylenedithiolato)trimethoxyphosphineiron(IV)

H. Miyamae, S. Sato, Y. Saito, K. Sakai and M. Fukuyama

CCDC reference: 1231511

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Neutron powder diffraction study of the intermediate-temperature form of lithium tantalum oxide

A. Santoro, R. S. Roth and D. Minor

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Triammonium orthoarsenate trihydrate

T. H. Hseu and T. H. Lu

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10-Methoxycarbonyldecyltriphenylphosphonium iodide

J. C. van Niekerk and L. R. Nassimbeni

CCDC reference: 1210125

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The hydrogen bonding of artinite

M. Akao and S. Iwai

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Refinement of pyroelectric lithium perchlorate trihydrate

S. Chomnilpan, R. Liminga and R. Tellgren

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2,3-Dimethyl-4a,9a-diaza-1,4,4a,9,9a,10-hexahydroanthracene-9,10-dione

C. Foces-Foces, F. H. Cano and S. García-Blanco

CCDC reference: 1210479

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Berylliumtellurat Be₄TeO₇

M. Trömel and Müllner Maetz J.

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1-Methylcytosine: a refinement

M. Rossi and T. J. Kistenmacher

CCDC reference: 1211430

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issue contents

December 1977 issue

research papers

short structural papers