Acta Crystallographica Section C
Acta Crystallographica
Section C STRUCTURAL CHEMISTRY

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STRUCTURAL
CHEMISTRY

Volume 48| Part 10

ISSN: 2053-2296

October 1992 issue

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inorganic compounds

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Structure of CuZr₂(PO₄)₃ by X-ray and neutron powder diffraction

I. Busserau, M. S. Belkhiria, P. Gravereau, A. Boireau, J. L. Soubeyroux, R. Olazcuaga and G. Le Flem

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A niobium silicophosphate belonging to the niobium phosphate bronze series: K₄Nb₈P₄SiO₃₄

A. Leclaire, M. M. Borel, J. Chardon, A. Grandin and B. Raveau

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Structure refinement of the semi-metallic oxide SrTl₂O₄: a neutron diffraction study

C. Michel, M. Hervieu, V. Caignaert and B. Raveau

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Redetermination of the structure of potassium tetranitropalladate(II)

A. J. Blake, R. O. Gould, B. F. G. Johnson and E. Parisini

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metal-organic compounds

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Structure of bis(thiourea)gold(I) bromide, [Au{SC(NH₂)₂}₂]Br

L. C. Porter, J. P. Fackler Jnr, J. Costamagna and R. Schmidt

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Structures of chromium(III) cyclam complexes. 3. Structure of trans-dichloro(1,4,8,11-tetraazacyclotetradecane)chromium(III) bromide

C. G. Dealwis, R. W. Janes, R. A. Palmer, J. N. Lisgarten, D. Maes, C. D. Flint and D. M. Gazi

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Structures of chromium(III) cyclam complexes. 4. Structure of trans-bromochloro(1,4,8,11-tetraazacyclotetradecane)chromium(III) bromide displaying structural enantiomorphism with the dibromo complex

T. K. Chattopadhyay, R. A. Palmer, J. N. Lisgarten, L. Wyns and D. M. Gazi

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Structure of a tetrahedral niobium oxo compound [Nb(OC₆H₃Ph₂-2,6)₃(O)]

J. S. Yu, P. E. Fanwick and I. P. Rothwell

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Structure of bis(hexafluoroacetylacetonato)bis(triphenylphosphine oxide)nickel(II)

J. R. Polam and L. C. Porter

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Structure of μ-dioxane-bis[(ethanol)bis(hexafluoroacetylacetonato)nickel(II)]

R. R. Romero, F. Cervantes-Lee and L. C. Porter

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Structures of racemic and meso (5,7,7,12,14,14-hexamethyl-1,4,8,11-tetraazacyclotetradeca-4,11-diene)nickel(II) perchlorate

D. J. Szalda and E. Fujita

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Structure of a permethylcyclopentadienyl-μ-tetramethylcyclopentadienylmethylene scandium dimer

S. Hajela, W. P. Schaefer and J. E. Bercaw

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A silicon-bridged bis(substituted Cp) yttrium complex

R. E. Marsh, W. P. Schaefer, E. B. Coughlin and J. E. Bercaw

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A bis(pyrazolyl)(bipyridyl)platinum complex

W. P. Schaefer, W. B. Connick, V. M. Miskowski and H. B. Gray

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Tetrabromo(1,4,7,10,13,16-hexathiacyclooctadecane)dimercury(II)

M. Herceg and D. Matković-Čalogović

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Structure of [Ca(triethylene glycol)₂]Cl₂.4H₂O

R. D. Rogers and A. H. Bond

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Mixed chelate complexes. III. Structures of (L-alaninato)(aqua)(2,2'-bipyridine)copper(II) nitrate monohydrate and aqua(2,2'-bipyridine)(L-tyrosinato)copper(II) chloride trihydrate

X. Solans, L. Ruíz-Ramírez, A. Martínez, L. Gasque and R. Moreno-Esparza

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organic compounds

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4-Iodo-2,2,6,6-tetramethylheptane-3,5-dione

S. Sans-Lenain, A. Reynes and A. Gleizes

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Stereochemical investigation of 2,3,4,6-tetra-O-acetyl-1-S-benzhydroximoyl-α-D-glucopyranose

V. Durier, H. Driguez, P. Rollin, E. Duee and G. Buisson

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Structures and absolute configurations of enantiomers of two local anaesthetics: (2S)-1-methyl- and (2R)-1-butyl-2',6'-pipecoloxylidide hydrochlorides

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Structure of 3-(p-chlorophenyl)-1-phenyl-1,3-propanedione enol

P. Gilli, V. Ferretti, V. Bertolasi and G. Gilli

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A urea with non-planar nitrogen-bonding geometry

A. C. Regan, J. D. Wallis and D. C. Povey

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Structure du chlorhydrate de (1R,2S)(3-hydroxy-3-m-hydroxyphényl-2-propyl)triméthylammonium monohydrate

L. Dupont, O. Dideberg, M. C. Pardon and J. L. Piette

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Structure of the lactonic adduct from 2-hydroxypinan-3-one and glycine

J. Lapasset, A. El Marini, M. L. Roumestant, Y. Vidal and P. Viallefont

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Structure du 2,3-dihydro-3-(2-hydroxyéthylthio)benzo[b]thiophène 1-oxyde, C₁₀H₁₂O₂S₂

D. Ginderow, J.-P. Mornon, I. Erdelmeier, P. Dansette and D. Mansuy

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Structure and conformation of photosynthetic pigments and related compounds. 4. Two crystal forms of a chlorin - rhodochlorin XV dimethyl ester

M. O. Senge, K. Ruhlandt-Senge and K. M. Smith

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Structure of sp-9-hydroxy-9-pivaloylfluorene, product of base-catalyzed autoxidation of ap-9-pivaloylfluorene

C. Y. Meyers, J. L. Tunnell, P. D. Robinson, D. H. Hua and S. Saha

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Structure of (E)-4-benzoylbutyramide oxime

J. K. Maurin, I. C. Paul and D. Y. Curtin

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Structure of 3-benzoylbenzamide oxime

J. K. Maurin, I. C. Paul and D. Y. Curtin

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Structures of two bufadienolides: telocinobufagin (3β,5β-dihydroxy-5β,14β-bufa-20,22-dienolide) monohydrate and 14α-artebufogenin (3β-hydroxy-15-oxo-5β,14α-bufa-20,22-dienolide)

G. Argay, A. Kálmán, B. Ribár, D. Živanov-Stakic and S. Vladimirov

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Structure of the antipsychotic drug 3-{2-[4-(6-fluoro-1,2-benzisoxazol-3-yl)-1-piperidinyl]ethyl}-2,9-dimethyl-4H-pyrido[1,2-a]pyrimidin-4-one (ocaperidone)

W. I. Jottier, H. L. De Winter, O. M. Peeters, N. M. Blaton and C. J. De Ranter

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short format (inorganic compounds)

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Refinement of the structure of boroleucite, K(BSi₂O₆)

D. Mikloš, Ľ. Smrčok, S. Ďurovič, D. Gyepesová and M. Handlovič

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short format (metal-organic compounds)

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Carbonyl(1-methyl-η⁵-cyclopentadienyl)bis(triphenylphosphine)manganese dichloromethane solvate

A. L. Rheingold, C. B. White, B. S. Haggerty, M. R. Terry and G. L. Geoffroy

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Structure of [2-(chlorodimethylstannyl)ethyl]diphenylphosphine selenide

H. Preut, B. Godry and T. N. Mitchell

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Dichlorotetrakis(pyridine)nickel(II)

R. E. Bachman, K. H. Whitmire, S. Mandal and P. K. Bharadwaj

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Structure of the μ-azido-dichloro(η⁵-methylcyclopentadienyl)titanium(IV) dimer

K. Kirschbaum and D. M. Giolando

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Structure of triphenyltin chloride-triphenylphosphine oxide (1/1) complex

S. W. Ng and V. G. Kumar Das

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Carbonatobis(1,10-phenanthroline)cobalt(III) perchlorate

C. A. McAuliffe, R. G. Pritchard, M. R. Bermejo, A. Garcia-Vazquez, A. Macias, J. Sanmartín, J. Romero and A. Sousa

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Structure of bis(trifluoracetamidinium) di-μ-chloro-hexachlorodioxodimolybdate(V)

R. Herbst-Irmer and E. Egert

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Tri-μ-chloro-bis(1,4,7-trithiacyclononane)dinickel(II) tetrafluoroborate acetonitrile solvate

A. J. Blake, M. A. Halcrow and M. Schröder

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short format (organic compounds)

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Structure of ethyl 8,9-dimethoxy-3-(4-methoxyphenyl)-10b-methyl-1-phenyl-4,5,6,10b-tetrahydro-1,2,4-triazolo[3,4-a]isoquinoline-5-carboxylate

F. Theobald, N. Rodier, K. Moustaid and B. Laude

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Ethanol complex of 1,3-diethoxy-p-tert-butylcalix[4]arene

K.-E. Bugge, W. Verboom, D. N. Reinhoudt and S. Harkema

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Structure du 8-chloro-11-(4-méthylpipérazin-1-yl)dibenzo[b,f]-1,4-thiazépine

L. Dupont, O. Dideberg, J. F. Liégeois and J. Delarge

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Structure of xindongnin B

J.-L. Wang, L.-J. Zhang, F.-M. Miao, H.-D. Sun and Y.-H. Gong

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Absolute configuration of (−)-α-acetylmethadol hydrochloride

J. L. Flippen-Anderson and C. F. George

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Structure of 3,6-diacetyl-8-benzoylantakyatriol

P. W. Baures, M. Miski and D. S. Eggleston

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Structure of 7-diethylamino-4-trifluoromethylcoumarin

K. Chinnakali, K. Sivakumar and S. Natarajan

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Structure of 3-tert-butyl-1-[(4-chlorophenyl)sulfonyl]-1-methylurea

M. Ghosh, A. K. Das, S. K. Mazumdar and G. Bocelli

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Structure of corydaline

B. Ribár, D. Lazar, P. Radivojević, P. Engel, O. Gašić and I. Kanyó

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Structure of cis,cis-4,6-diphenyl-2-(2-propenyl)-1,3-dioxa-2-phosphorinane 2-oxide

D. H. Hua, D. Roche, S. N. Bharathi, X. Wu and P. D. Robinson

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Structure of a p-nitrobenzoyl praziquantel analogue

R. A. Toscano, M. Rubio, R. Cetina and B. M. Pérez-Ibarra

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Structure of 10-acetyloxy-10-methyl-9(10H)-anthracenone

T.-Y. Lin, Y.-L. Mao and C.-M. Chuo

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Structure of 8,10-diacetyl-2,4,6-trinitro-2,4,6,8,10-pentaazabicyclo[5.3.0]decane

R. Gilardi, J. L. Flippen-Anderson and C. F. George

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Structure of a bicyclic guanidinium nitrite salt

A. Meetsma, E. van Aken and H. Wynberg

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Structure of 1,1-dibromo-2-phenylseleno-3-p-tolylcyclopropane

J. Zukerman-Schpector, E. E. Castellano, J. V. Comasseto and H. A. Stefani

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Structure of a chiral intermediate in the synthesis of (+)-19-epiajmalicine

V. M. Lynch, J. W. Corbett, S. F. Martin and B. E. Davis

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2-Menthyl (2-hydroxyphenyl)glycolate

G. Bocelli and A. Cantoni

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Structure of tris(5-acetyl-3-thienyl)methane-n-hexane (3/1) inclusion compound

H. M. Roos and J. L. M. Dillen

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N,N-Diethyl-6-(hydroxyimino)-α-methyl-1-cyclohexene-1-acetamide

P. J. S. S. van Eijk, W. Verboom, D. N. Reinhoudt and S. Harkema

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N,N-Diethyl-2-[2-(hydroxyimino)cyclohexylidine]propanamide

P. J. S. S. van Eijk, W. Verboom, D. N. Reinhoudt and S. Harkema

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regular structural papers (metal-organic compounds)

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Dimeric nickel(II) carboxylates and a silanecarboxylate: [Ni(Me₃CCOO)₂(2,5-lutidine)]₂, [Ni(MePh₂CCOO)₂(quinoline)]₂.2CHCl₃, [Ni(Me₂PhCCOO)₂(quinoline)]₂, [Ni(Me₃CCOO)₂(2-ethylpyridine)]₂, [Ni(Me₃CCOO)₂(2-picoline)]₂ and [Ni(MePh₂SiCOO)₂(Ph₃P)]₂

M. Morooka, S. Ohba, M. Nakashima, T. Tokii, Y. Muto, M. Kato and O. W. Steward

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Structure of [2-(fluorodimethylstannyl)ethyl]diphenylphosphine oxide

H. Preut, B. Godry and T. Mitchell

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Structure of a dichromium(II) complex with bridging betaine ligands, [Cr₂(O₂CCH₂NMe₃)₄(OH₂)₂][ZnCl₄]₂.2H₂O

W. Clegg, B. P. Straughan and A. R. Yusoff

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regular structural papers (organic compounds)

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Structure of 2-[(4-methylphenylimino)methyl]-1-nitrobenzene

G.-Y. Yeap, H.-K. Fun, S.-B. Teo and S.-G. Teoh

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Structure of an oxonium salt crystal complex

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Structure of a polydentate alkoxide ligand, cis-tetrahydroxytetramethylcyclobutane

M. M. Olmstead, J. L. Hobbs and R. P. Planalp

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Structure of the allene C₃₉H₃₂P₂²⁺.2CF₃O₃S⁻

A. Bram, H. Burzlaff, D. Hadawi and H.-J. Bestmann

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{2S-[2α,3α,3aβ,6β(R*),7α,7aα]}-6-(3-Benzyloxy-2-propyl)-2-hydroxy-2,3,7-trimethylhexahydro-4H-furo[3,2-c]pyran-4-one, a rearrangement product of pyranone derivatives in the tirandamycin A series

M. Parvez, M.-T. Lin and P. DeShong

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1,8-Dichloro-5-oxa-10-azatricyclo[5.3.1.0^3,8]undecan-9-one: structure of a hydrolysed Diels-Alder addition product

M. G. Barlow, R. G. Pritchard, L. Sibous and A. E. Tipping

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Oxonium (R)-O-acetylmandelate

G. Ferguson, J. F. Gallagher, R. Fullwood and D. Parker

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short communications

Acta Cryst. (1992). C48, 1912